Hair testing research round-up
In a world full with mirrors and Instagrammable opportunities, the way hair looks is generally at the top of the list of beauty priorities. It's no wonder, then, that haircare products account for a significant portion of the beauty market. Today's producers must attain product consistency and high standards, as well as novelty value and noticeable outcomes, if they are to succeed in keeping customers coming back for more.
The science of texture analysis has a wide range of applications in the haircare industry. With its compressive and tensile capabilities, the TA.XTplusC Texture Analyser can apply specially designed test techniques to examine an unrivalled range of physical qualities. These test methods can be used to evaluate claims about product performance by quantitatively testing the effects on hair.
It's a faced-paced, attention-seeking, secretive game where patents are necessary to protect new innovations and hair care novel inventions. It’s no wonder that the Texture Analyser has been found in the following patents and research to substantiate haircare claims.
Three-point Bending Tests on Hair
Compositions and Methods for Treating Hair Patent from L’Oreal
The goals of many hair styling compositions include to hold or fix the hair in a particular shape, to impart or increase volume of the hair, and/or to smooth the hair, e.g. to decrease or eliminate the appearance of frizz. Drawbacks associated with current products include a sticky or tacky feel, and styled hair that is stiff and/or “crunchy” (i.e. the film is hard and brittle resulting in a crunching feel or sound when the hair is touched), which is undesirable for most consumers. This patent describes compositions containing at least two latex polymers, wherein at least one latex polymer is a film-forming polymer. The composition is capable of forming a film having certain properties on a substrate.
Process for Styling Human Hair Patent from BASF
Hair styling products containing water or ethanol soluble polymers are very popular products in today's cosmetic market. Such products typically involve a liquid or wax/gel-like composition which is applied on wet or dry hair to obtain a certain long-lasting hair style. They can be produced as aerosol sprays, sprays, mousses, gels, waxes, serums or other textures. This patent describes a polymer formulation and styling process to allow for lower damage to heat treated hair.
Styling polymers and their influence on mechanical properties of hair styling gel Research from Dabur Research and Development and Lubrizol, India
Many hair styling products are available on the market in the form of hair spray, gels, mousses, creams, waxes, lotions and pomade. Among these hair gels plays a vital role in hair styling segments. Bend tests are useful to estimate the stiffness of the hair after gel application, as do high humidity curl retention experiments, which assess style longevity. The formulation developed in this publication delivered high humidity resistance, excellent curl retention, superior hold and no flakes. The measurement of stiffness through bending was used to classify the gel into four categories – mild, gentle, strong and super hold.
Measuring hair friction
Composition for conditioning keratin fibers Patent from L'Oreal
Keratin fibres, in particular the hair, is cleansed and treated with many cosmetic regiments to improve its look, colour and style. However, these various regiments can remove the hair's natural oils and impart structural damage to the hair. This patent describes a composition and cosmetic process for caring for keratin fibres. They used their TA.XTplus Texture Analyser to measure the frictional force between the hair and a polyurethane pad, and from this the friction force reduction percentage after treatment was calculated.
Hair Conditioning Composition having Improved Rinse Properties Patent from Unilever
Reducing the amount of water that is used in everyday tasks and activities, such as washing of hair, reduces the energy required to process and deliver it to homes, businesses and communities. This patent presents a conditioning composition that comprises a conditioning base and a hydrophobically modified anionic polymer that can be used in the treatment of hair to reduce the amount of water required to rinse without reducing the conditioning benefits on the hair. They found that when a consumer rinses conditioner from his/her hair, he/she will stop rinsing when a satisfactory constant level of smooth feel is reached (the “rinsed friction plateau”). The composition of the invention enables the consumer to reach his/her rinsed friction plateau sooner, when compared to a composition comprising the same ingredients but without the hydrophobically modified anionic polymer, thus causing him/her to stop rinsing and therefore consume less water.
Evaluation of the surface properties of hair with acoustic emission analysis Research from Ashland Specialty Ingredients
The tactile sensation of hair is an important consumer‐perceivable attribute. There are limited instrumental options to measure the haptic properties of hair. This study introduced a novel technique using the acoustic emissions produced when skin comes in contact with dry hair in a stroking motion. Acoustic emission profiles were generated allowing the monitoring of the acoustic response at distinct frequencies. They used their TA.XTplus Texture Analyser to determine the stroking force of the middle and index fingers over the hair tress. This study introduced a cutting‐edge method to reproducibly evaluate the surface properties of hair. Different types of hair geometry produce unique acoustic profiles as do hair types that experience harsh damaging treatments. This is also a very practical and efficient way to evaluate the degree of protection or conditioning of the fibre.
Hair tensile properties
Ionic liquid and ultrasound-assisted extraction of chestnut shell pigment with good hair dyeing capability Research from Huazhong Agricultural University
To effectively extract the pigment from chestnut shell in a green and efficient way, an eco-friendly and efficient method based on ionic liquid ultrasonic assisted extraction (IL-UAE) was established. The physico-chemical properties of hair dyed with chestnut shell pigment extracted by IL-UAE were compared with those extracted by conventional organic solvents, using (amongst other methods) tensile testing of the hair samples.
Other hair property measurements, such as hair combing and hair volume, are also available.
MEASURING HAIR VOLUME WITH THE VOLSCAN PROFILER
See how Ashland, USA scientists Lidia Kulcsar, David Streuli, Roger L. McMullen, Coralie Alonso, Michael Franzke and Richard Giles have been using the Volscan Profiler to compare mousse samples containing Guar HPT Chloride or PQ-11 to evaluate volume.
View the full article and results
To review the typical types of tests used in the hair and hair product industry for texture measurement visit our Hair and Hair Product testing page
See how haircare industry leaders use texture analysis to get ahead of their competition
Alternatively request our articles that gives an overview of all of these methods for hair and hair product testing
Texture analysis of materials from upcycled sources
Today’s dominant production model creates vast amounts of waste. Byproducts and waste generation have an impact on the environment, economy, and society. These have an impact on the environment by contributing to greenhouse gas emissions. Many of these biomaterials are discarded and end up in municipal landfills or being burned to kill fungi and parasites.
However, engineers and designers are finding increasingly imaginative ways to repurpose industrial by-products into valuable new materials. Examples include newspaper pressed into rolls that can be sawn, sanded and varnished like ordinary wood, roofing tiles incorporating polymer waste and bioplastic made from by-products of the potato industry.
Upcycling, also known as creative reuse, is the act of transforming waste materials, obsolete or undesirable things into new resources or products of higher quality, such as those with artistic or environmental value. Many companies and researchers are focussing efforts into the area of upcycling.
The following are examples of recently published research studies in this area incorporating Texture Analysis:
By perceiving by-products as valuable resources that can be turned into new, value-added goods while simultaneously bringing social and environmental advantages, upcycling organisations are helping to normalise the concept of waste reduction.
Why is texture so important to personal care and skincare products?
Consumers today expect to be wowed by a personal care product, and texture is crucial in this process. It occurs in the first instance due to the aroma, which is the primary criterion for first product purchase and subsequent brand loyalty. The second factor is touch, which is a sensory factor. Humans are connected to the world through their senses, thus it's critical to provide them with a positive sensory experience when using a product. People no longer solely value a product by how effectively it performs but they now particularly like it when a texture changes when it comes into contact with their skin or hair. Brands have recognised this and have directed their formulators to develop new components that combine the strength of many textures to increase the consumer's enjoyment of the product. To create textural transformations formulators working swiftly to align formulations with this latest sensory trend by using particular components and scientific understanding to change the texture of a cosmetic product that stands out in the market.
The latest innovations in skincare
Pressed, solid, whipped — the latest skin-care formulas for serums and creams are designed to deliver more active ingredients to skin and to hydrate it better than a typical lotion can. On top of that, they feel fantastic.
These serums start as a fairly solid balm, which then melts into a lotion. One specific ingredient, a polymer called a rheology modifier, is responsible for this transformation, causing the thick formula to become flowable when you apply pressure by massaging it into skin, Once you've rubbed the serum in fully, it shifts back to a thin balm, leaving a nice, cushiony feel and an effective barrier that holds moisture in. The result: You get the hydration of a thick balm without its greasy side effects.
When you swipe a solid serum stick across your face, the heat from your skin causes it to melt and then sink in instantly. As solid sticks are formulated with little to no water, they're able to contain more or higher levels of active, effective ingredients which means that they remain stable with fewer preservatives.
Whipped formulas are all about the sensory experience. Biomimetic ingredients, for example, create a cloud-like consistency and enable the delivery of extracts that boost the skin's own natural moisture.
Our suggested tools for measuring these textures include penetration tests for solid/pressed formulations and back extrusion tests for semi-solid or whipped cosmetics.
Hemispherical probe, conical probe and Back Extrusion Rig for testing skincare products on a Texture Analyser
The latest articles on skincare product texture
But don’t take our word for how important texture is to personal care and cosmetics products. Here are a few non-biased articles for you to peruse:
Latest research discoveries
Make-up clumps, bumps and collapses are the three factors that determine how well make-up has performed. A study by researchers from LG Household & Health Care Seoul aimed to reduce these three factors by using amphiphilic substances to increase the affinity between the skin and the make-up layer. In addition, it aims to evaluate the improvement of the make-up layer by developing an objective make-up layer evaluation method. Experiments were performed in an attempt to increase the affinity between the skin and the make-up layer by minimising the difference in surface energy between the two. Multiple types of artificial skin (leather and bio-skin) were used and treated to form the liquid foundation layer. Qualitative evaluation of the make-up layer was conducted by analysing the surface, cross-section, and fracture area of the make-up layer. They then used their TA.XTplus Texture Analyser to simulate muscle movement with constant force. It has been confirmed that through this method, the quality of consumer experience related to make-up satisfaction can be improved. Read more
Discover the typical types of physical property measurement used in the cosmetics and skincare industry
Request our articles that give an overview of all of the methods available for cosmetic and skincare product testing
Read our Blog posts about Cosmetics and Skincare Texture Analysis
See how Cosmetic Industry Leaders use Texture Analysis to get ahead of their competition
Advances in petfood: Texture analysis in research
The soaring demand for protein poses a real challenge, because current available supplies just can't keep up. This gap between protein supply and demand is expected to continue to expand as the world population reaches 9 billion people by the year 2050 (and as global pet ownership also increases).
From alligator, kangaroo, buffalo and brushtail possum in dog and cat treats petfood companies have cleverly catered to growing consumer demand for ever more exotic and novel sources of protein. Just as people are seeking to try new types, and increase the levels, of protein in the foods they eat, they are doing the same for their pets' foods, thanks to ongoing humanisation.
As animal proteins become scarcer for pet food applications, emerging proteins may soon fill the niche. Many plant-based proteins have been widely used in human and animal nutrition for years such as soybeans, peas, lupin beans, potatoes, wheat and corn. Others are just now starting to become popular and widely available.
See example texture analysis research at Saturn Petcare and State University of Campinas, Brazil:
Upcycling is a new word for something the pet food industry has done for a long time, using human food products that would have otherwise gone to waste. Upcycled pet food ingredients use existing materials, especially otherwise discarded foods like misshapen vegetables, to make a value-added item.
See example texture analysis research at Universidade Estadual Paulista (UNESP), Brazil:
Fortified and functional foods are packaged foods and beverages that have been enhanced with additional health components and/or nutrients in order to provide a nutritional benefit. Pet treats are given to dogs to strengthen pet and owner bonds and as a reward but it is essential to understand the functionality of the raw materials and relate their impact on animal health and acceptance of the pet and the pet owner.
See example texture analysis research at Kansas State University, USA:
Currently, the number of approved veterinary medicines are limited, and human medications are used off-label. These approved human medications are of too high potencies for a cat or a small dog breed. Therefore, there is a dire demand for smaller doses of veterinary medicines. 3D printing could potentially be used to manufacture personalised doses for animals at the point-of-care.
See example texture analysis research at Åbo Akademi University, Turkey:
One alternative protein source gaining attention is insects, and is already spilling over into petfood. For people who are not comfortable eating them directly, insects still have a role to play in addressing climate change and making agriculture more sustainable. Using insects as a feed source for farm animals has been happening already and is a lot less costly for the environment than traditional feeds.
See example texture analysis research into animal feed containing insects:
However, unlike our farm animals, our pets may be all too fussy to switch unless the palatability of the new petfood is up to their liking. As the purchaser of their food, consumers loyalty is affected when the pet finds their new food not to their liking. Whilst it would not be clear whether that was due to taste or texture, the right food texture should be high on a formulators list of priorities. This is when you need to compare the texture of original ‘well liked’ petfoods with their reformulated counterpart to see whether you have created a textural match.
For more information visit our Petfood Applications page to see our range of test methods online or request a copy of the article ‘Texture Analysis of Pet Food and Accessories’, covering a wide range of test method ideas.
How texture analysis can advance personalised medicine
What is Personalised Medicine?
Imagine your medicine being tailored to your exact needs based on your gender, size, genetics and desired drug form.
The traditional medical approach comprises a ‘one-size-fits-all’ application of drugs. This does not consider interpatient variability and, has long been known, may result in significantly different therapeutic outcomes among patients. The ability to provide the optimum dosage and apply an ‘individual’ approach to patients has gained increasing interest due to ongoing development in the field of human genome research and new potential manufacturing technologies, i.e. 3D printing. Providing genetic information on an individual patient level improves decision-making regarding the right active pharmaceutical ingredient, dose, and time required for a specific patient resulting in fewer adverse effects and superior treatment outcomes.
In addition to making medical decisions based on patient data and lifestyle factors, personalised medicine can involve taking into account the personal preferences of a specific patient. A solid oral dosage form can be tailored according to personal preferences related to e.g., size, colour, shape, and taste, which can be particularly important for acceptability among children and patients with swallowing conditions. To date, the administered dose is typically tailored by manipulation of the marketed formulation by splitting or crushing tablets into smaller pieces or opening capsules. However, such manipulation of solid oral dosage forms is not accurate and may lead to day-to-day variability of the administered dose and thus result in undesired over- or under-dosing. Manipulations of solid oral dosage forms can also alter the properties of the dosage form with potentially dangerous outcomes such as dose dumping of a sustained release dosage form or destroying the pH-sensitive coating resulting in release of the active drug at the wrong site in the gastrointestinal tract.
Conventional fixed procedure and process parameters e.g., tableting, involve processes that are well understood and have well-established regulatory pathways but lack the flexibility needed for manufacturing personalised dosage. The U.S. Food and Drug Administration (FDA) are encouraging pharmaceutical companies to implement modern and innovative manufacturing technologies and processes, such as printing technologies, which are flexible and enable production of advanced dosage forms with high accuracy, to solve this unmet need. The ability to manufacture personalised dosage forms is forecasted to advance treatment outcomes by enabling patient-tailored medicines that have improved efficacy, safety, compliance, and accessibility.
How can 3D printing help?
3D printing enables production of innovative and complex solid oral dosage forms, drug delivery devices, and medical devices with regards to the geometrical shape and complex inner structures that are not easy or impossible to attain with conventional manufacturing methods. The potential ease of manipulation of the printed solid dosage form makes 3D printing attractive for use in personalised medicine and would allow tailored solid oral dosage forms to be produced on-demand, in small volumes, with a limitless number of product designs and various personalisation features, e.g., patient-tailored drug content, drug release profile, and customized functionality, according to the patients’ needs. This may result in improved treatment outcomes lowering the societal burden associated with poor treatment outcomes that are costly for society.
How can Texture Analysis help?
Different printing technologies exist, e.g. fused deposition modelling, semisolid extrusion 3D printing, inkjet printing which require vastly different properties of the starting materials, involving solid, semisolid, and liquid states of matter. Each one will potentially produce a solid dosage form that has different mechanical properties that will ultimately affect the effectiveness of the drug. For a medicine to be effective and safe the active pharmaceutical ingredient (API) needs to be delivered in a desired, safe, and unvarying way to the intended target in the body. Pharmaceutical development aims to define the design space, specifications, and manufacturing requirements to achieve this. This will, amongst other vital measurements, need extensive knowledge of the resulting mechanical properties of the 3D printed forms which will need to be measured in order to ensure the medicine will be effective on the basis of the contribution of properties to correct tablet breakdown at the intended target.
How texture of 3D printed pharmaceuticals can be measured
Materials for printing should have adequate rheological properties that can be easily extruded and maintain their shape. Any materials that are proposed for 3D printing will require ‘printability’ testing to ensure they possess the correct rheological properties or consistency. Formulations will need to be assessed for their extrudability and the resulting printed products measured by way of a compression test to ensure mechanical expectations are matched. The fracture and bending characteristics of a tablet may also be a necessary assessment.
Typical compression, extrusion and bending tests on a Texture Analyser
Here are specific research examples of where texture analysis has already been applied in this way:
How a Texture Analyser can assess 3D printer base powder flowability
Texture Analysis can also be put to use at other stages in the 3D printing process, not just for the measurement of final product properties. For example, the properties of the base powder used in Selective Laser Sintering affect the sintering process as well as the properties of the final product. Powder flow is one of these properties. As each new layer of powder is swept onto the sintering bed, the layer should be uniform and of the correct thickness and distribution. A Powder Flow Analyser (PFA) is a very useful add-on to a Plus Connect Texture Analyser to help measure these flow properties.
The PFA proves an accurate and reliable method of measuring the flow characteristics of dry and wet powders, with capability to measure cohesion, caking and speed flow dependence as well as bulk density and other properties.
The Powder Flow Analyser on the TA.XTplusC Texture Analyser
As the benefits of personalised medicine are becoming evident, the conventional way of developing and manufacturing dosage forms needs to be adapted to moreover consider the personalisation aspect. This requires a paradigm shift from manufacturing large batches with a fixed drug content to manufacturing processes that allows for easy alteration of the dosage form. This is where Texture Analysis needs to be employed.
To read more about how texture analysis can be applied to 3D printing, pharmaceutical product property measurement and assessment of powder flow, request the following articles:
Texture Analysis in Research: Gluten-free Products
Since the days when rice flour and tapioca were the go-to gluten-free substitutes for wheat flour and other gluten-containing grains, gluten-free formulations have come a long way. However, consumers' expectations for gluten-free product development are becoming increasingly complex. This means that gluten-free product formulators and marketers must recognise that consumers care about more than just gluten; they care about nutrition, flavour, and the assurance that the product is gluten-free.
While people with coeliac disease and gluten sensitivity had few or no gluten-free options in consumer packaged products 20–30 years ago—and only limited options 10 years ago—gluten-free solutions are now available in practically every segment of the market. However, the two areas where there is still some attention needed are quality—does the product taste good and have a good texture. Gluten-free products are improving, but some are still just a highly starchy imitation of something that used to include fibre, protein, and substance. Consumers are increasingly starting to realise that if formulators don't match up the nutritional attributes of the original ingredients, it can have negative health consequences. Technology, novel ingredients, and active consumer interaction are the keys to success.
There are a number of recent research publications dealing with these issues that use the Texture Analyser as a tool to assess the effects on texture:
Cookies and Cakes
Through the production of gluten free bakery products, stakeholders of the food industry are striving to serve the needs of coeliac patients as widely as possible with a continuously increasing product range ensuring the right nutrient intake without compromise on textural quality.
Texture Analysis is a mandatory stage in the Research and Development of ingredient-substituted bakery products, when texture can be altered by the addition of different quantities of ingredients, and must be measured after each iteration of ingredient or process modifications.
Fortification of Bakery Products and its Effect on Texture
Fortification, the addition of certain bioactive or functional ingredients to food products to enhance their nutritional and therapeutic value, allows consumers to improve their nutrition without having to alter their eating habits. Bakery products are an excellent candidate for fortification. According to Euromonitor International, baked foods make up one of the largest packaged food categories, with global baked foods retail sales volume predicted to reach about 177 million tons by 2022.
Fortification was historically used to prevent malnutrition. However, it is more commonly used today to improve wellbeing and general health, thereby adding value to a manufacturer’s products. The nutrients most often included are iron, zinc and B vitamins: folic acid, niacin, riboflavin, thiamin, vitamin B12 and vitamin B6. These vitamins and minerals have been shown to support life-long health. Several prevent anaemia, and folic acid reduces the risk of birth defects of the brain and spine.
“Different age groups and lifestyles have different nutritional requirements, so it is important to know who the target consumer is before developing a concept,” said Nathan Pratt, R.&D. scientist, nutrition, Kerry Ingredients. “For example, children need iron, calcium, vitamin A and vitamin D for optimal growth and development, but many kids do not get enough of these, so they are great candidates for fortification into foods kids eat frequently.”
The alteration or addition of ingredients frequently affects a product’s textural characteristics. There have been countless publications of research into the use of fortification in the bakery industry using Texture Analysers, in both academic and industrial settings. Some examples of the most recent research are outlined below.
The Effect of Moringa oleifera Leaf Powder on the Physical Quality, Nutritional Composition and Consumer Acceptability of White and Brown Breads – Fortifying popular, affordable, but nutrient-limited staple foods, such as bread, with Moringa oleifera leaf powder (MOLP) could contribute significantly to addressing under-nutrition, especially protein and mineral deficiencies, which are particularly prevalent among a large proportion of populations in sub-Saharan African countries.
Utilisation of pineapple pomace powder as functional ingredient in bread – Pineapple processing generates major by‐products in the peel (30–42 %, w/w); followed by the core (9–10%); stem (2–5%, w/w); and crown (2–4%, w/w). These by‐products account for 50% (w/w) of total pineapple weight and are a potential source of important compounds such as sucrose, glucose, fructose, cellulose, fibre, bromelain and phenolics. Peel flour has very good prebiotic potential to support probiotic bacteria in the gut. Fermentable sugars and other nutrients make pineapple waste extracts excellent media to produce enzymes, single cell proteins, bacterial cellulose and organic acids. Waste can also be utilised to produce vinegar and vanillin and to extract bioactive compounds that can be used in food, pharmaceutical or allied industries. The waste also has the potential to act as alternative source of energy.
Protein enrichment of wheat bread with the marine green microalgae Tetraselmis chuii – Impact on dough rheology and bread quality
Marine green microalgae are a sustainable source of high-quality protein. However, due to their green pigmentation and composition of volatiles, their incorporation into food products is a challenge. Ethanol treatment of algae may be a feasible strategy to address the sensory and structural challenges that hinder incorporation of algae into foods at levels that can potentially confer nutritional benefits.
Effect of psyllium fiber addition on the quality of Arabic flatbread (Pita) produced in a commercial bakery – Lack of fibre in diets leads to higher incidence of obesity and metabolic syndrome, not only in adults but also in children. Higher intake of soluble fiber products coming from psyllium husk, provides better protection against these noncommunicable diseases but is not without challenge to the formulation without affecting consumer acceptability of the staple Arabic flatbread in Kuwait. This study discovered that incorporation of psyllium husk did not adversely affect the objective color of crumb or overall consumer acceptability, and produced Arabic flatbread with softer texture, better flexibility (folding) and superior eating quality.
Effect of Taro (Colocasia esculenta) Enrichment on Physicochemical and Textural Properties of Cake – Taro is a plant widely produced in tropical areas for its underground corms and it is used mainly as a vegetable. Its physicochemical, sensory properties and health benefits suggest its use in value-added products such as cake where a lower gluten content is required. Taro-supplemented cake shows higher mineral and fibre content, however, reduced caloric value whilst improving texture and sensory characteristics in comparison to wheat cake.
Nutritional, antioxidant, and quality characteristics of novel cookies enriched with mushroom (Cordyceps militaris) flour – Fortification of C. militaris flour can improve the functional quality of cookies by significantly enhancing the phenolic contents and antioxidant compared to plain wheat cookies. Their supplementation could provide the consumers a novel cereal-based product with health-promoting benefits.
Development of a healthy cookie to promote toddlers’ brain development: Brainy Bites – Brainy Bites will serve as a great snack for toddlers at home, nurseries or for travelling. The cookie will be accepted in the market and would be a better choice of snack for toddlers as it contains no added sugar and salt, and contains ingredients such as raisins, almonds and chia seeds that may help in the brain development among toddlers.
Texture Analysis is a mandatory stage in the Research and Development of fortified bakery products, when texture can be altered by the addition of different quantities of ingredients, and must be measured after each iteration of ingredient or process modifications.
To view a wide range of test solutions for bakery products visit our Bakery Product Testing page
Reducing Fat in Food and the Effect on Texture
Delicious desserts, mouth-watering canapes, mind-blowing buffets….no doubt you will have experienced these during the festive season and have started noticing the consequences. Your consumers will have put on some unwelcome pounds too and will be looking for several solutions to remove them. It’s likely that they will turn to the reduced-fat versions of their preferred food choices. However, texture plays a large part in consumer enjoyment and expectations of textural attributes remain high. When reformulating your products you will be looking for change that show as little impact as possible. Understanding the impact on texture and the potential implications of these texture changes is crucial in ensuring new product launches aren’t a miss with consumers.
Reducing the fat content and energy value of a food product implies the application of an adequate fat substitute. Ideal fat substitutes should have all the functional characteristics of lipids, but also lower energy value, preferably 0 kcal/g. The functional properties that a fat substitute should have are sensory properties (odour and taste) and rheological properties (viscosity, consistency, texture).
Around the world there have recently been several pieces of research published in the areas of dairy, bakery and meat products – all known for their popular high calorie offerings and all looking for solutions to offering a lower fat counterpart. Here’s how they’ve applied their Texture Analyser:
A modified plant sterol, beta-sitosteryl oleate, was incorporated into a reduced-cholesterol butter to improve its physicochemical properties. The reduced-cholesterol butter was comparable to regular butter with respect to its consistency and melting properties and could be made into sticks. In addition to the reduced-cholesterol butter, this product could provide the foundation for new products blending butter and oils to create other low-cholesterol, reduced saturated-fat products, possibly in stick form. Read more
In the bakery and snacks industry the increased demands of healthy natural foods represent a challenge for food processors. Chia gel as fat substitute for producing low fat cake has been found to produce a product that maintains its physicochemical properties and nutritional quality as well as consumer acceptability.
With consumers constantly searching for healthier options in their food, bakery manufacturers are looking to improve the nutrient profile of their products. So how about: Use of glycosylated wheat protein in emulsions and its application as a fat replacer in microwave cakes? Or, Bamboo Fiber as a Substitute for Fat and/or Sugar in Cookies?
Can a structured emulsion (fat in water‐fiber system) substitute saturated fat in cookies without hampering their quality? Replacing fat and saturated fat in baked goods without affecting their quality characteristics is a challenging task but the use of structured emulsion might be a valuable alternative to develop a potentially healthier product with acceptable sensory properties. And how about the Reduction of saturated fat in chocolate by using sunflower-hydroxypropyl methylcellulose based oleogels as a partial cocoa butter replacer in chocolates?
In the meat industry the use of different sources of materials (mostly from plants) as a fat replacer to ensure palatability required by consumers is not an easy task. Many different ideas have been investigated in a wide range of meat products:
Plant-based oil inks that imitate the texture and melting behavior of traditional animal fats using 3D printing have also been developed. Fat analogues containing coconut oil could be texturised at temperatures lower than those required for their soybean oil counterparts.
Consistent, objective measurement is vital for informing reformulation and new product development, in addition to maintaining high quality standards. To read more about the texture of reformulated food products, request our article
Texture Analysis in Research: Incorporation of Insects as Ingredients in the Bakery Industry
Back in December 2019, Roberts Bakery in Norwich were the first UK bakery to launch a loaf of bread containing cricket flour. The uptake from other bakeries has been slow in the UK; customers will take some convincing before they overcome their trepidation to eat insects. However, it is likely that insects will become a regular part of our diets in years to come.
Insects such as crickets provide a protein source with a high feed-conversion efficiency rate (an animal's capacity to convert feed into increased body mass). They also require much less water than traditional protein sources such as poultry or cattle. Health benefits of insect consumption include their high antioxidant power and chitinous fibre content, as well as the upside of a higher protein content in whichever food they are added to. The challenge lies in introducing insect protein into the Western diet. This has to begin with ingredient replacement in existing foods, one example of which is bakery products, as these act to familiarise consumers with insect-based food.
The texture of a bakery product can be altered after the addition of insect ingredients, particularly when they are there to replace something else. Biscuit/bread firmness might change, measured using a penetration/compression test; bread dough properties can be affected, measured using a Dough Inflation System; or final product volume may be altered, which a manufacturer would be able to monitor using a Volscan Profiler.
There have been countless publications of research into the use of insects in the bakery industry using Texture Analysers, in both academic and industrial settings. Some examples of the most recent research are outlined below:
And using the Texture Analyser with a Kieffer rig, three point bend rig or cake penetration:
Texture Analysis is a mandatory stage in the Research and Development of insect-incorporated bakery products, when texture can be altered by the addition of different quantities of ingredients, and must be measured after each iteration of ingredient or process modifications. Review all of the probes and fixtures that can be used for the texture measurement of bakery products.
Latest developments in the creation of new materials
A large portion of the plastic produced worldwide is used as packaging material, and only around 68% of the packaging bought by consumers is recycled, resulting in several tons of plastic ending up in the oceans each year. Because of these problems, the use of biopolymers as packaging material has become increasingly popular over the last few decades in the need to shift towards a greener alternative. Although natural biopolymers could be attractive alternatives to conventional plastic, generally, films made from biomaterials generally have low mechanical strength and poor barrier properties – compromising functional properties on the safety of the product being packaged. However, these properties could be improved by the addition of certain materials (e.g. chitosan or alginate) or by crosslinking, such is the work of many recent and ongoing research projects, for example that are using their Texture Analyser to explore the mechanical suitability of such ideas:
Plastic straws contribute to waste and result in the release of greenhouse gases in their manufacture. Despite this, they provide a superior sensory experience compared to other options. Scientists from Cornell University have been investigating alternative biodegradable and reusable drinking straws as alternatives to single-use plastic. This study contains a review of aspects of this experience, along with consumers' motivations for using straws. They measured the durability of straws soaked in water, using their TA.XTplus Texture Analyser to perform three-point bend tests. Read more
Meanwhile, in the Czech Republic scientists are looking into Plastic Cutlery Alternative: Case Study with Biodegradable Spoons.
Fungal mycelia are versatile, highly productive and sustainable sources for biocomposites to replace conventional plastics. However, with only very few fungal strains that have been characterised, numerous strains still remain unexplored as potential competitors against traditional non-biodegradable materials. Moreover, the functionality of mycelium composites at commonly occurring, challenging ambient conditions such as changing humidity and temperature is not well characterised. Researchers from the University of Helsinki evaluated the properties of the fungal composite material produced by novel fungal strains, including Trichoderma asperellum and Agaricus bisporus, grown on oat husk and rapeseed cake after oil pressing. They used their TA.XT2i Texture Analyser to perform compressive tests. The results showed that the mycelium composites were hydrophobic and strong, particularly when grown on rapeseed cake. A. bisporus grown on rapeseed cake exhibited increased stiffness after humidity was successively increased and decreased. The moisture-resistance of these novel mycelium composites is encouraging for novel sustainable material solutions.
Cellular glass is a type of insulation that is composed of crushed glass and a material such as limestone or carbon. Because glass is a large part of its composition, it possesses some of the same advantages of glass. There are many applications for cellular glass. It can be specially shaped for insulating objects such as pipes or tanks or used to produce insulation panels for structures. Other applications include cold storage and flotation devices. Work that is being carried out in this field of materials using a Texture Analyser includes:
Other materials are also being progressed providing such characteristics as shape recovery, compression strength, adhesiveness, hardness or rigidity – the mechanical properties depending upon the purpose of the material:
In the fast-paced world of electronics the constant redevelopment of mobile phone technology calls for the assessment of materials with properties that provide new functional opportunities and experiences for the consumer. With recent development of display-relating technologies, display devices transformable at the stage of use such as folding, rolling in a roll shape or stretching like a rubber band have been researched and developed. These displays may be transformed into various shapes, and therefore, may satisfy demands for both a larger display at the stage of use and a smaller display for portability. However, existing adhesive compositions for a foldable display have had problems in that, even when satisfying such a folding reliability condition, delamination and panel breakage occur when conducting a dynamic folding test at −20° C, a severe condition among conditions allowing an actual folding test. A patent has recently been released by LG that provides satisfying reliability conditions without causing problems such as delamination and breakage even at −20° C when conducting a folding test while maintaining properties of existing adhesive compositions for a foldable display such as reliability conditions and adhesion properties at room temperature and high temperature. They used their TA.XTplus Texture Analyser to perform peel tests.
Due to the empirical or imitative way that the Texture Analyser range can be applied, it is called upon time and time again for use in innovative areas of industry such as the creation and development of new materials. Unbound by fundamental or standard methods and analysis options, the Texture Analyser provides the flexibility of method development unavailable in other materials testing instruments. For this reason, it is found in countless recent patents applications where testing solutions for the measurement of properties of new materials are required for mechanical testing problems which cannot be assessed by applying rigid, old-fashioned standard method approaches. To discover more innovative material applications go to our Innovative Material Physical Property Measurement page
Texture Analysis in the Advancement of Medical Products
Tissue engineering now plays an important role in the replacement, repair, maintenance, or enhancement of tissue function. The tissue engineering relates to the use of a “scaffold” combining with cells and biologically active molecules into functional tissues. The goal of tissue engineering is to generate new viable tissue by assembling functional constructs that are suitable for tissue formation. Many biomaterials have been applied to produce a scaffold which is an artificial structure that acts as a template for tissue formation and also as an optimum microenvironment for cell attachment, migration, proliferation and differentiation. The harvested cells attach onto the scaffold, so that it will migrate, multiply, grow and develop into tissue. In order to provide the proper microenvironment for the cells, the scaffold must be biocompatible and non-toxic with the cells. It must be biodegradable and have suitable mechanical strength, surface chemistry and high porosity. For example in the following research:
Three-dimensional (3D) printing technology is also a revolutionary breakthrough in the era of personalised medicine. 3D printing brings numerous advantages to fulfil personalised treatment, especially for the manufacture of pharmaceutical implants, tissues and oral drugs. Implantable delivery systems can be fabricated with the desired shape and structures to fit, for example, a tumour-resected site. The porosity and surface area can be easily altered by computer-aided design (CAD) to achieve predictable release kinetic. Rapid prototyping makes it possible to real-time print customised implants for individual patients at a low cost.
Recently, there have been many research achievements in the 3D bioprinting sphere that employ a Texture Analyser as part of medical research:
Currently, transdermal drug delivery systems (TDDS) are an attractive alternative drug delivery pathway for oral administration and hypodermic injection, as they are painless, convenient, and may increase the bioavailability of the drugs. Moreover, TDDS may provide the controlled delivery of a drug through the stratum corneum for local or systemic approaches. TDDS provides several advantages, such as the avoidance of drug destruction in the digestive tract and hepatic first-pass effect, a reduction of gastrointestinal side effects, a single application for multi-day therapy, the possibility of rapid cessation due to an uncomplicated removal, and the possibility of providing an accurate dose of drugs. Drug-in-adhesive patches take advantage of close contact by the attachment of the patches and the stratum corneum, the barrier to drug transportation through the skin, to deliver the drugs into the skin or the blood circulation. Pressure-sensitive adhesives (PSAs) are one of the most significant components in a transdermal system. PSAs are used for skin adhesion and as a matrix for drugs and other excipients. PSAs can impact the properties of transdermal patches, such as drug permeation, adhesive properties, and physicochemical properties. PSAs should be safe for the skin, adhere quickly and strongly to the skin, and be detachable without pain and leave no residue on the skin. A Texture Analyser is typically used to measure a range of adhesive properties to characterise transdermal patches. For example in the following research:
The search for an ocular drug delivery system that could provide long-acting effects without a detriment to the anatomy and physiology of the eye remains a challenge. Properties that may need to be measured and controlled for this drug delivery method include tensile/compressive strength and mucoadhesion. For example in the following research:
The medical industry is becoming heavily reliant on the TA.XTplusC Texture Analyser as a tool for the measurement of all types of physical/mechanical properties. See a wider range of test and measurement possibilities in this field.
The Volscan Profiler in food research
The Volscan Profiler was originally designed for use with bakery products. However, its use has exploded into other industries in the past few years, both food- and non-food-based. Not only is volume critical to bakery products, it is also an important physical property of agricultural products, meat, fish and packaging.
Agricultural products have the characteristic of being ‘low value added’ when compared with other industrial commodities. As a result, the application of state-of-the-art technology to the agricultural sector has been slow; it is only in relatively recent times that various up-to-date techniques have reached the point of practical implementation.
Previous volume methods may have involved simple water displacement; however, this method produces one volume value that is usually manually recorded and so attracts operator inaccuracy with no data archiving system for future retrieval. Fluid displacement techniques are also unsuitable for porous materials.
The Volscan Profiler is a benchtop laser based scanner that measures the volume, density and dimensional profiles of products with maximum dimensions of 600mm long and 380mm diameter, with a typical test time of less than 60 seconds. As well as volume, numerous related parameters are automatically measured, such as product height, width, length and surface area. It also enables the rapid 3-dimensional digitisation of products that can be archived and then treated mathematically to yield detailed dimensional information for immediate use or future retrieval.
This instrument rapidly provides the accurate data essential in the fields of both Quality Control and Product Development. There have been countless publications since the launch of the Volscan Profiler over ten years ago showing its versatility in both academic and industrial settings. Some examples of the most recent Volscan research in the wide food industry are outlined below:
Comparison of explosion puffing drying with other methods on the physicochemical properties and volatiles of yam (Dioscorea opposita thunb.) chips through multivariate analysis – Researchers from Liaoning University used their Volscan Profiler to measure the bulk volume of yam chips.
Multivariate analyses of the physicochemical properties of turnip (Brassica rapa L.) chips dried using different methods – Scientists from Liaoning University also used their Volscan Profiler to measure the bulk volume of their turnip chips.
Quality and protein degradation of golden pompano (Trachinotus blochii) fillets during four drying methods – Researchers from Hainan University used their Volscan Profiler to measure the volume of fish fillets.
The impacts of vacuum microwave drying on osmosis dehydration of tilapia fillets – Scientists from Hainan University used their Volscan Profiler to measure tilapia sample volumes.
Relationship between quality characteristics and skin color of ‘Fuji’ Apples (Malus domestica Borkh.) – Scientists from Korea Food Research Institute used their Volscan Profiler to measure the volume and weight of apples.
Antioxidant profile of thinned young and ripe fruits of Chinese peach and nectarine varieties – Researchers from Shenyang Agricultural University used their Volscan Profiler to measure fruit volume.
Evaluation of current and emerging techniques for measuring eggshell integrity of the domestic fowl – Researchers from the University of Kentucky used their Volscan Profiler to measure egg dimensions.
In a fast-paced food industry, rapid product measurement and provision of automatically calculated quality control pass or fail benchmarks is key to manufacturing intelligence and success. The Volscan Profiler has been helping manufacturers to achieve these aims for over a decade.
Texture Analysis in Research: 3D Printing in Bakery and Snack Products
3D printing has made a large impact in many sectors, but its entry into the food industry has not been a simple journey. The first difficulty to overcome is the range of food products that have until now been printable. Additionally, the properties of finished 3D printed products require a large amount of research (texture and rheology as well as colours and general appearance) and development along with the printing conditions to achieve them (such as temperature, speeds and raw materials).
However, the potential benefits of incorporating 3D printing into food manufacture are significant and far outweigh any teething problems.
• Time-saving: labour costs can be saved, as there is no need for manual operation once the print has been launched.
• Food waste reduction: food products can be printed on demand, so perishable products can be manufactured as and when their need arises.
• Personalisation of nutritional content: this allows food to meet dietary requirements, or to be fortified.
• Customisable appearance: intricate, imaginative shapes can be created, giving freedom to chefs and manufacturers. This includes tailoring food to special events, or to incorporate customers’ names or images.
There have been countless publications of research into 3D printing in the bakery and snack industries using Texture Analysers, in both academic and industrial settings. Some examples of the most recent research are outlined below.
A rheological approach to 3D printing of plasma protein based doughs – Scientists from the University of Seville have used their TA.XT2 Texture Analyser to perform Texture Profile Analysis.
Designing Mechanical Properties of 3D Printed Cookies through Computer Aided Engineering – Researchers from the University of Leuven used their TA.XTPlus Texture Analyser to perform compression measurements. Finite element modelling was used to establish the relationship between the Young modulus of 3D printed cookies with a honeycomb structure and their structure parameters.
Influence of Selected Product and Process Parameters on Microstructure, Rheological, and Textural Properties of 3D Printed Cookies – Scientists from the Indian Institute of Technology Kharagpur have been using their TA.XT2i Texture Analyser to measure cookie hardness by penetration. The hardness of the baked cookies was influenced by printing temperature, fill density, and water butter ratio of 3D printed cookie dough and their interactions. This study shows the importance of considering the specific ingredient and printing parameters to develop high quality 3D-printed cookies.
LF-NMR intelligent evaluation of rheology and printability for 3D printing of cookie dough pretreated by microwave – Researchers from Jiangnan University have been investigating low-field nuclear magnetic resonance intelligent evaluation of rheology and printability for 3D printing of cookie dough pretreated by microwave. They used their TA.XT2 Texture Analyser to measure the texture properties of dough.
Investigation on evaluating the printable height and dimensional stability of food extrusion-based 3D printed foods – Scientists from Jiangnan University used their TA.XT2 Texture Analyser to measure texture characteristics. Results indicated that the zero shear viscosity and Young's modulus of food inks were linearly related to the 3D printable height of samples within a certain range, and storage modulus (G′) was linearly correlated to the shape stability of printed samples. This study would provide some universal applicable information on the relationship between 3D printable height, shape stability, and food ink's material properties.
Programmable texture properties of cereal-based snack mediated by 3D printing technology – Scientists from the University of Foggia used their TA.XTplus Texture Analyser to measure hardness of the snacks. The hardness of the snacks reduced from 289 N to 84 N following the reduction of the relative density, from 0.569 to 0.401. The results open interesting perspectives of creating novel foods with desired texture addressing specific requirements, or novel sensory/satiety perception.
Texture Analysis is the first step in the Research and Development of 3D printed bakery and snack products, when texture can be unpredictable and must be measured after each iteration of ingredient or process modifications.
How to test Microneedles and latest use of Texture Analysis
Microneedle (MN) arrays are minimally-invasive devices used to penetrate the skin’s outermost layer, the stratum corneum, the principal barrier to topically-applied drugs. They are widely used in a range of applications including cosmetics and pharmaceuticals. Their use involves a simple, cheap, safe, and effective technique requiring minimal training. Microneedles were originally used as a collagen induction therapy for facial scars and skin rejuvenation, and still are, but are also now widely used in the form of patches as a transdermal delivery system for therapeutic drugs and vaccines.
There have been countless publications of research into the properties and use of microneedle arrays for drug delivery using Texture Analysers, in both academic and industrial settings. These are the main areas of research:
– The compression of arrays into a known soft substrate such as animal skin or synthetic analogues, assessing the penetration force required for each array
– The measurement of the force applied by a human subject to an array on a soft substrate, generally performed on the calibration platform of the Texture Analyser
– The properties of the array backing material, measured using a tensile test
– The compression of arrays into a hard substrate to a known force. Needle strength is an important characteristic of arrays. Needles should be strong enough to be inserted into the skin without failure. The needle stiffness may be measured from the force-displacement graph and in some cases an ultimate strength may be measured as a breaking point on the graph. Most commonly, the percentage change in microneedle height due to buckling or blunting is assessed by measurement in a calibrated optical or electron microscope. The compression of needles into a metal base is a very different method from their insertion into skin. This test is simply used to compare different batches of arrays and confirm consistency of manufacture, or to assess the effect of different manufacturing processes on needle strength.
Some examples of the most recent research are outlined below.
Dissolving Microneedles for Intradermal Vaccination against Shigellosis – Researchers from the University of Navarra used their TA.XTplus Texture Analyser to perform compression tests to assess percentage change of needle height as well as insertion force into a substrate.
3D printed microneedles for anticancer therapy of skin tumours - Scientists from the University of Greenwich have used their TA.HDplus Texture Analyser to measure the ability of MN arrays to penetrate skin.
A novel 3D printed hollow microneedle microelectromechanical system for controlled, personalized transdermal drug delivery & Optimisation of Design and Manufacturing Parameters of 3D Printed Solid Microneedles for Improved Strength, Sharpness, and Drug Delivery – Researchers from the University of Kent have used their TA.HDplus Texture Analyser to measure the ability of the MNs to pierce porcine skin and determine the penetration force.
Successful application of large microneedle patches by human volunteers – Scientists at Queen’s University Belfast have been researching the efficiency of large microneedle patches for transdermal drug delivery, with the intention of using the technology in clinical drug delivery. The needle strength of these patches was measured using an axial compression test to a set force on a TA.XTplus Texture Analyser, with the array attached to the moving test probe of the Texture Analyser using double-sided adhesive tape. The texture analyser was also used for the controlled application of microneedle arrays to folded thin film artificial skin, for the purpose of inspecting the number of holes per depth once the sheet was unfolded.
Pullulan microneedle patches for the efficient transdermal administration of insulin envisioning diabetes treatment – Scientists from the University of Aveiro have used their TA.XT2 Texture Analyser to perform compression tests for needle strength as well as penetration tests into a substrate.
The assessment of the mechanical properties of microneedle arrays is a mandatory stage in their Research and Development. These properties may be altered by changes to raw materials, the drug being delivered, and the manufacturing process used. They must be measured after each iteration of ingredient or process modification.
Texture Analysis: A Tool in the Fight of HIV
HIV (human immunodeficiency virus) is a virus that damages the cells in the immune system and weakens a person’s ability to fight everyday infections and disease. While AIDS cannot be transmitted from one person to another, the HIV virus can. There is currently no cure for HIV, but there are very effective drug treatments that enable most people with the virus to live a long and healthy life. In the three decades since the first cases of AIDS were reported, investments in basic, biomedical, behavioural, and social science research have led to numerous HIV prevention interventions and life-saving treatments. Texture Analysis has an important role in this research, specifically in the improvement of drug delivery systems. We’ve included some examples of Texture Analysis in HIV research in recent years.
Researchers from Queen’s University Belfast have been investigating mechanical testing methods for drug-releasing vaginal rings. Vaginal rings (VRs) are currently marketed for contraceptive or hormone regulation purposes, and investigationally have been widely reported for delivery of antiretrovirals to reduce HIV transmission. To date, there is no national or international standard for the mechanical testing and minimum performance characteristics of any VR based products. They used their TA.XTplus Texture Analyser to perform 1000 cycle compression tests on multiple samples in a purpose-built holder as well as twisting measurements. Read more
Meanwhile, at Complutense University of Madrid, scientists have been undertaking a large amount of research into mucoadhesive vaginal drug delivery systems, including films, tablets and gels. Researchers have been investigating mucoadhesive vaginal films based on HMPC and zein as novel formulations to prevent sexual transmission of HIV. Although vaginal films were initially developed for a fast release of the drug, with a suitable formulation they can also be useful for sustained release. The latest strategies for the prevention of the sexual transmission of HIV have moved towards sustained-release dosage forms, so films may be an effective strategy that could also improve the patient’s comfort. They used their TA.XTplus Texture Analyser to measure the resistance and elasticity of Tenofovir sustained-release vaginal films. The film formulation developed here proved not only to have excellent mechanical properties, but was also able to release TFV in a sustained manner for 120 hours and remain attached to biological tissues throughout this time. This film could be an interesting option for the prevention of sexual transmission of HIV. Read more
Complutense University of Madrid researchers have also been investigating dapivirine bioadhesive vaginal tablets based on natural polymers for the prevention of sexual transmission of HIV. Young sub-Saharan women are a group that is vulnerable to the sexual transmission of HIV. Pre-exposure prophylaxis through vaginal microbicides could provide them an option for self-protection. Dapivirine has been demonstrated to have topical inhibitory effects in HIV, and to provide protection against the sexual transmission of this virus. They used their TA.XTplus Texture Analyser to measure the bioadhesion of gel samples. Find out more
Researchers from the same group have been investigating chitosan-based mucoadhesive vaginal tablets for controlled release of the anti-HIV drug tenofovir. Vaginal microbicides have the potential to give women at high risk of contracting HIV the option of self-protection by preventing the sexual transmission of the virus. They used their TA.XTplus Texture Analyser to measure the hardness of tablet samples. Read more
Lastly, from Complutense University of Madrid, scientists have been researching smart freeze-dried bi-gels for the prevention of the sexual transmission of HIV by accelerating the vaginal release of tenofovir during intercourse. Sub-Saharan African women are still at risk from the human immunodeficiency virus (HIV), and sex with men is the main route of transmission. Vaginal formulations containing antiretroviral drugs are promising tools to give women the power to protect themselves. They used their TA.XTplus Texture Analyser to perform mechanical tests on bigel samples. Find out more
Scientists from the Girijananda Chowdhury Institute of Pharmaceutical Science have also been researching mucoadhesive vaginal gels. They have been looking at the development and evaluation of mucoadhesive nanogels of nevirapine for vaginal application, for the treatment of HIV infection. Mucoadhesive nanogels have gained greater attention as an alternative to conventional gels in the last decade. They are easier to handle and administer due to their lower viscosity at room temperature. However, the high viscosity of the nanogels at room temperature can minimise the chance of gel leakage. Consequently, developing a mucoadhesive nanogel of nevirapine may increase the residence time of the formulation. They used their TA.XTplus Texture Analyser to perform mucoadhesion tests on different gels. Find out more
In an entirely different approach, researchers from Mercer University have been developing a transdermal delivery system for tenofovir alafenamide, a prodrug of tenofovir with potent antiviral activity against HIV and HBV. Tenofovir alafenamide (TAF) is an effective nucleotide reverse transcriptase inhibitor that is used in the treatment of HIV-1 and HBV. Currently, it is being investigated for HIV prophylaxis. Oral TAF regimens require daily intake, which hampers adherence and increases the possibility of viral resistance. Long-acting formulations would significantly reduce this problem. They used their TA.XTplus Texture Analyser to perform adhesion tests on developed transdermal patches. Find out more
How Texture Analysis is progressing the development of even better gluten-free products
The global demand for gluten-free products is expanding and continues to be a significant technological challenge for the bakery industries. One of the principle challenges is producing gluten-free baked goods and pasta with similar textural quality to the gluten-loaded counterparts.
The market demand of gluten-free (GF) baked goods is expanding. Despite the health halo associated with GF food category, commercially available GF cereal-based foods are often characterised by lower nutritional quality than their gluten-containing counterparts, having lower dietary fibre, protein and resistant starch (RS) contents, along with enhanced starch digestion rates and extents.
Plenty of research has therefore been conducted to ameliorate the nutritional profile of GF foods and one of the possible strategies is the partial replacement of common GF-flours with novel nutrient-dense raw materials. Legume flours, dairy proteins, fruits and vegetable-based powders, along with fibre sources and other GF materials have been added at different inclusion levels in GF baked goods aiming to enhance their technological and nutritional profiles. However, reformulation of baked goods can affect dough rheology and staling rates of the finished products and ultimately affecting such properties as crust and crumb hardness.
There are a number of recent research publications dealing with these issues that use the Texture Analyser as a tool to assess the effects on texture on bakery products:
Through the production of gluten free products, stakeholders of the food industry are striving to serve the needs of celiac patients as widely as possible with a continuously increasing product range ensuring the right nutrient intake without compromise on textural quality.
To read more, request our article ‘Applying Texture Analysis to Gluten-Free Products’.
Texture Analysis: A Tool in the Fight against Cancer
“More than 40 years after the war on cancer was declared, we have spent billions fighting the good fight. The National Cancer Institute has spent some $90 billion on research and treatment during that time. Some 260 nonprofit organisations in the United States have dedicated themselves to cancer — more than the number established for heart disease, AIDS, Alzheimer’s disease, and stroke combined. Together, these 260 organisations have budgets that top $2.2 billion.” (Dr Margaret Cuomo, A World Without Cancer)
We’d like to share several examples of recent cancer research from around the world, and the role that Texture Analysis has to play.
Much of the role of Texture Analysis in cancer research involves the development of drug delivery systems, due to their need for precise physicochemical properties. Drug delivery is the method of delivering drugs to their site of action within the body, with the goal of achieving a therapeutic outcome. Microneedle research is a common application of Texture Analysis. Microneedles are microscopic applicators used to deliver drugs across the skin and other barriers with benefits compared to traditional hypodermic needles, such as the possibility for controlled drug release.
Read about how researchers from the University of Greenwich have been investigating 3D printed microneedles for anticancer therapy of skin tumours using their TA.HDplus Texture Analyser.
Over the past few decades, mucosal drug delivery has received a large amount of attention. Mucoadhesive dosage forms may be designed to enable prolonged retention at the site of application, providing a controlled rate of drug release where necessary. Additionally, the application of dosage forms to mucosal surfaces can be particularly useful for drug molecules not amenable to the oral route.
Read about how scientists from the University of Campinas have been investigating hyaluronic acid in the intestinal tract, including its influence on structure, rheology and mucoadhesion on the intestinal uptake in rats using their TA.XTplus Texture Analyser to investigate the mucoadhesive properties of the different HA formulations.
Meanwhile, over at the University of Reading, scientists have been researching chitosan/β-glycerophosphate in situ gelling mucoadhesive systems for intravesical delivery of mitomycin-C and employing their TA.XTplus Texture Analyser for mucoadhesive measurement. The development of mucoadhesive in situ gelling formulations for intravesical application may improve the therapeutic outcomes of bladder cancer patients. Read more
A researcher from the same group in Reading researched more widely novel mucoadhesive chitosan based formulations for drug delivery to the urinary bladder for their PhD thesis. The intravesical route was chosen as the exemplar transmucosal mode of drug delivery due to the limited therapeutic efficiency of conventional bladder cancer formulations. Drug carriers with improved mucoadhesive properties may prolong drug residence in the bladder. They used their TA.XTplus Texture Analyser to evaluate the ability of the chitosan or CHIGP solution to pass through a catheter via a syringe. These excipients were found suitable for use in formulating affordable transmucosal dosage forms with superior mucoadhesiveness for a variety of biomedical applications. Read more.
Medicated Chewing Gum for Head and Neck Cancers
Researchers from the University of Louisiana at Monroe have been investigating mechanical characterisation and dissolution of chewing gum tablets (CGTs) containing compressed Health in Gum® and Curcumin/Cyclodextrin Inclusion Complex. Curcumin chewing gums could be therapeutically beneficial if used by the head and neck cancer patients. However, high curcumin loading in chewing gums is needed to achieve the desired therapeutic effect. Preparing gums with high drug load is nonetheless challenging because of the negative impact of solids on their masticatory properties. Find out more about how they employed their TA.XTplus Texture Analyser.
Dermal Application of Drugs for Skin Cancer
Ethosomes are a novel carrier system used for the delivery of drugs that have a low penetration through the skin and other body barriers. They are soft vesicles made up of Phospholipids, Ethanol and water. Because of their unique structure, ethosomes can efficiently encapsulate and deliver highly lipophilic molecules and hydrophilic drugs into the skin. For this reason, they are particularly suitable drug carriers for skin-related diseases, such as skin cancer.
Researchers from Jamia Hamdard have been investigating fisetin loaded binary ethosomes for management of skin cancer by dermal application on UV exposed mice. They used their TA.XTplus Texture Analyser to measure gel texture. Find out more...
3D Cancer Models
Modelling the behaviour of tumours can help with the understanding of cancer initiation, growth, and migration, and the key role of the tumour microenvironment on these processes. Cancer research has considerably progressed with the improvement of in vitro study models.
Researchers from the University of Stavanger have been modelling 3D cancer growth and extracellular matrix properties in vitro. Cancer can be defined as loss of normal behaviour of cellular components, losing tissue organisation and giving rise to a tumour microenvironment (TME). Increased matrix stiffness, strain and elevated interstitial fluid flow and/or pressure of the extracellular matrix (ECM) in TME is characterised as the cause of initiation and progression of tumourigenesis. Find out more about this research and how they used their TA.XTplus Texture Analyser to perform mechanical testing on collagen samples.
Gene therapy holds the potential to rapidly advance the treatment of cancer. Gene delivery is a necessary step in gene therapy for the introduction or silencing of a gene to promote a therapeutic outcome in patients. There are many different methods of gene delivery for various types of cells and tissues. Gene therapy efficacy can be improved by prolonging the release of nucleic acid drug payload for sustained, long-term treatment.
At Queen’s University Belfast scientists have been investigating the influence of alginate backbone on efficacy of thermo-responsive alginate-g-P(NIPAAm) hydrogel as a vehicle for sustained and controlled gene delivery. They used their TA.XTplus to measure the injection force of samples. Read more
Symptom Management and Palliative Care
In addition to these applications focussed on efficient and effective drug delivery and the specifics of tumour structure and properties, Texture Analysis has a large part to play in developing ways of keeping patients more comfortable, particularly when it comes to end of life or prolonged hospital care. These applications are also relevant to many other illnesses.
Dysphagia (difficulty swallowing) is a common symptom of cancers, either caused as a side effect of treatment, or because a tumour disrupts swallowing and the passage of food. This can cause problems with discomfort, weight loss and dehydration in cancer patients. Food and liquid texture play very important roles in the care of people with dysphagia, and so there have been countless publications characterising readily-available foods as acceptable to dysphagia sufferers. There have also been many Texture Analysis investigations into thickeners and gelling agents as additives to liquids to promote a controlled swallowing process and add to the patient’s comfort.
Pressure sores are caused by pressure applied to the same area of skin for a long time period, and are consequently common during end of life care. When the patient cannot be moved due to aggravation of other symptoms, barrier creams and films are invaluable in alleviating discomfort. Physical properties of these products, such as cream spreadability or film strength, are measured using imitative or fundamental methods using a Texture Analyser.
A large number of drugs are still administered via hypodermic needle despite the progression of research into other drug delivery routes.
The properties of the syringe and needle system can be investigated using a Texture Analyser, including the puncture force of the syringe tip, and the injection force of each combination of syringe and contents. The tailoring of all of these components can help create a more comfortable experience for the patient.
Chemotherapy and end of life dehydration can both cause a dry mouth. This can be uncomfortable, but there are products that can help alleviate this symptom such as artificial saliva in spray, gel, lozenge or pastille form. Texture Analysis is a key stage in the development of these products to ensure they are the correct consistency for provision of comfort, but also last a long time in the mouth to reduce the need for reapplication.
To find out more about how Texture Analysis can be applied to cancer research, request our article 'Texture Analysis: A Tool in the Fight against Cancer'.
The Volscan Profiler in Bakery Research
Loaf volume is of paramount importance to bread quality evaluation. It is a vital aspect of the consumer’s perception of value as in bread and other leavened goods, higher volume for a given weight is invariably associated with a more aerated crumb and superior texture.
For a baker or bread manufacturer, each batch of flour has to be evaluated by test baking to ensure that bread is made to a uniformly high quality. One component of this quality control is measurement of the volume of the bread, which can give information relating to the density of the bread crumb and the strength of the gluten in the flour. This volume information can then be used to modify the dough mix used in bread production to produce bread of the appropriate quality. This procedure is important, not only for the inherent qualities of the bread, but to ensure that the selected dough-piece weight produces a loaf of the correct size for the standard tins used in the baking process.
The baked product must also be capable of being handled by automatic slicing machines and packed into standard sized bags. It is therefore important to have a precise and rapid method for the measurement of the volume of bread loaves, enabling control and monitoring of bread-making conditions and manufacturing operations.
The Volscan Profiler is a benchtop laser based scanner that measures the volume of bread and bakery products with maximum dimensions of 600mm long and 380mm diameter, with a typical test time of less than 60 seconds. As well as volume, 19 related parameters are automatically measured, such as product height, width, length and weight. It also enables the rapid 3-dimensional digitisation of products that can be archived and then treated mathematically to yield detailed dimensional information for immediate use or future retrieval.
This instrument rapidly provides the accurate data essential in the fields of both Quality Control and Product Development. Compliance with the standard method AACC Method 10-16.01 provides further reassurance for operators with preference for the use of standard methods. There have been countless publications since the launch of the Volscan Profiler over ten years ago showing its versatility in both academic and industrial settings. Some examples of the most recent Volscan research in the bakery industry are outlined below.
Researchers from Sejong University have been investigating turanose as a sugar alternative in a frozen dough system, including their rheology, tomography and baking performance. They used their TA.XTplus Texture Analyser to measure tensile properties and their Volscan Profiler 600 to measure specific loaf volume. Read more
Researchers from the Technical University of Munich have been investigating water absorption capacity as a determination of the functionality of vital gluten releated to specific bread volume. Vital gluten is often used in baking to supplement weak wheat flours and improve their baking quality. Even with the same recipe, variable final bread volumes are common, because the functionality differs between vital gluten samples also from the same manufacturer. To understand why, the protein composition of ten vital gluten samples was investigated as well as their performance in a microbaking test depending on the water content in the dough. Read more
A patent has recently been released by BASF, entitled 'Lipase Enzymes'. Several different enzymes can be used for making bread, for example lipases have been known to improve the stability and volume of the bread. However, the industry still needs a lipase that improves volume, stability, tolerance, reduces or eliminates the additive diacetyl tartaric acid esters of monoglycerides. This patent explored lipase enzymes that meet or exceed these industrial requirements. They used their Volscan Profiler to measure volume as well as specific volume. Read more
Scientists from Manisa Celal Bayar University have been researching the use of persimmon powder in gluten-free cakes with determination of their physical, chemical, functional and sensory properties. Nutritious snack foods are of great importance for celiac people. This study investigated the effects of partial substitution of sugar with persimmon powder as a source of sugar, in gluten-free cake formulation. They used their Volscan Profiler to measure volume, specific volume and density. Read more
A patent has recently been released by KU Leuven, entitled 'Wholemeal Bread with Reduced FODMAP Content'. Dietary habits are believed to play a major role in pathogenesis of Inflammatory Bowel Syndrome (IBS) and a diet low in specific short-chain carbohydrates has been shown to markedly alleviate IBS symptoms in numerous cases. This patent presents a method for reducing fermentable oligo-, di-, and monosaccharides and polyols (FODMAP) levels in grain-based food products by addition of K. marxianus to the food making process. They used their Volscan Profiler to measure bread volume. Read more
In a fast-paced baking industry, rapid product measurement and provision of automatically calculated quality control pass or fail benchmarks is key to manufacturing intelligence and success. The Volscan Profiler has been helping manufacturers to achieve these aims for over a decade.
Powder Flow Analysis and Examples in Research
Almost every manufacturing industry has to deal with powders and granules at some stage during production. Depending on the nature of your powders, you will have different testing priorities.
There are three main test methods programmed into Exponent software for Powder Flow Analysis: caking, cohesion and powder flow speed dependency (PFSD), as well as variations such as cohesion measurement at four speeds.
Each test begins by default with two conditioning cycles to remove any user loading variation and to normalise the powder column after filling. Bulk density measurement has also been programmed into each of these sequences when the user chooses to use their split vessel, which sweeps the powder off the bulk down to a set line after conditioning. Additionally, the addition of a Powder Caking and Consolidation Rig allows the assessment of the sample’s caking behaviour after consolidation.
Caking behaviour in powders is typically undesirable and can be very difficult to measure. Understanding a powder's propensity to cake in advance is enormously useful for decisions regarding powder formulation, production before scale up, powder blending, handling, packaging, storage and transportation.
Caking is the tendency of a powder to form large agglomerates during storage and transportation. The tendency of a powder to cake is closely related to its cohesiveness and generally a powder that is cohesive will also form a definite cake during the caking test. The strength of the cake will depend on a number of factors such as packing efficiency, particle to particle interactions and moisture content i.e. humidity. Understanding the caking properties of a powder are important as most powders will be stored in hoppers or silos, or transported at some point in the production process. A powder that cakes easily and forms a strong cake may not discharge easily from a silo when required.
This test gently compacts the powder column to a user programmed force, then slices back to the top of the column with minimum disturbance, before recompacting. This is repeated for the programmed number of cycles and the rotor blade then slices the compacted cake. The cake height is measured at the beginning of each cycle.
Cake height ratio trend for a range of samples
Scientists from Universiti Putra Malaysia have been researching banana powder production via foam mat drying using caking strength. Read more
Scientists from Erciyes University (Turkey) have been researching powder caking and cohesion behaviours of coffee powders as affected by roasting and particle sizes, using principal component analyses for flow and bioactive properties. Read more
Cohesiveness is the tendency for particles of powder to cling together and agglomerate (form larger clusters of particles). The Powder Flow Analyser measures this cohesion characteristic by moving the blade in such a way as to lift the powder. A more cohesive powder will cling to itself and to the blade therefore reducing the force exerted on the base of the vessel. This is shown in the plotted data by a large negative force.
This quick analysis allows repeatable quantification of the cohesiveness of a bulk solid. Test results can be used to compare the sample being tested with previously analysed product, to assess if it is more cohesive or more free flowing. A Cohesion Index is determined that characterises the flow behaviour of the product from extremely cohesive to free flowing.
Researchers from Erciyes University have also been investigating the influence of sucrose reduction and starch type on bulk and powder properties of ready-to-use powdered dessert. Find out more
Scientists from the University of Zagreb have been researching the optimisation of the foam mat drying process for the production of cocoa powder enriched with peppermint extract. Read more
Powder flow properties may change with increasing or decreasing flow speeds. For example, a powder may become more resistant to flow as it is forced to flow faster or it may become more free-flowing as the flow speed increases. This issue can lead to under filling, for example, as a result of process changes to meet increase output demand. The Powder Flow Analyser measures this characteristic by assessing the work needed to move the blade though the powder at increasing speeds.
An evaluation of the flow stability of the powder is made by comparing the work needed to move the blade though the powder (compaction coefficient) at the start of the test compared to the work required to move the powder at the same speed at the end of the test. Powders that flow freely will transfer very little resistance through the powder column in either a downward or an upward direction. Conversely, poorly flowing powders exhibit substantial amounts of force in either direction.
Compaction coefficient trends with increasing tip speed for a range of samples.
Scientists from the Medical University of Gdansk have been investigating the use of novel tools for the assessment of powders and granules flow properties and for the analysis of the minitablets compression process. The purpose of this study was to apply rheological measurements to assess the flow properties of powders and granules and to compare the results with the standard pharmacopeial tests. Read more
The Powder Caking and Consolidation Rig
Many powder difficulties run into by manufacturers are due to the effects of storage, with the powder settling, caking and consolidating over time and under its own weight. The tendency of a powder to cake can give important data about the properties of the powder after storage and transportation. The formation of strong cakes may lead to issues with discharge of powders from storage hoppers or silos and may also impact on customer perception of products – as it could appear that the product is less voluminous than stated.
The effects of time and pressure on a powder’s flow properties can be assessed using the Powder Caking and Consolidation Rig. This rig is designed for location on a Powder Flow Analyser, allowing the assessment of the sample’s caking behaviour after consolidation.
Using this rig, the sample is prepared by filling a static consolidation tube to a chosen volume or weight. A compaction weight is introduced into the tube and allowed to rest on the powder column under controlled environmental conditions for a given period of time after which the sample is tested using the PFA blade. The area under the curve in the mid-section of the graph is taken as the work to break the cake. The greater this value, the stronger the cake.
Researchers from Lovely Professional University (India) have been investigating moisture sorption isotherms and quality characteristics of onion powder during storage as affected by sprouting using this test. Read more
Stable Micro Systems offer a large range of testing possibilities for your powders on top of Powder Flow Analysis. These include Unconfined Yield Stress, Powder Vertical Shear, an Indexable Powder Compaction Rig, High Tolerance Powder Compaction for tabletting research and Granule Compaction.
To read about ‘Measuring Powder and Granule Properties to anticipate problems’ using the Powder Flow Analyser and a wide range of other powder measuring tools for the Texture Analyser, request the article here
Texture Analysis: A tool for developing new food packaging from byproducts (waste)
By-products and waste generation are having an impact on environmental, economic, and social sectors. To the environment, these contribute to Green House Gas (GHG) emissions. Many of these biomaterials are not utilised and end up in municipal landfills where they create serious environmental problems due to microbial decomposition and leachate production. In some cases, the by-products are burned to remove fungi and parasites. From the economic point of view, the adverse impact is due to the costs related to the handling of solid waste in landfills. Moreover, the management of large amounts of different degradable materials poses a challenge.
However, there is an increasing need for biodegradable, environmentally friendly and functional food-packaging materials. In this regard, proteins obtained from agri-food industry by-products may become a promising and sustainable (less impact, valorisation) source of such materials.
Research into uses of Fruit waste
Agricultural production and agro-industrial processing generate a high amount of by-products and waste. Fruit by-products such as bagasse, peels, trimmings, stems, shells, bran, and seeds account for more than 50% of fresh fruit and have at times a nutritional or functional content higher than the final product. Fruit and food waste is also generated by damage during transportation, storage, and processing. The growing popularity of fruit juices, nectars, frozen and minimally processed products has also increased the production of by-products and wastes in recent years.
Scientists from the University of Aveiro (Portugal) have been investigating the tailoring of surface properties and flexibility of starch-based films using oil and waxes recovered from potato chip byproducts. Agrofood byproducts may be exploited as a source of biomolecules suitable for developing bioplastic materials. In this work, the feasibility of using starch, oil, and waxes recovered from potato chips byproducts for films production was studied. They used their TA.HDi Texture Analyser to perform tensile measurements on films according to standard ASTM D882. Potato chip industry byproducts were revealed to have thermoplastic and hydrophobic biomolecules that can be used to efficiently develop biobased plastics with improved surface properties and flexibility. Read more
Researchers from the Federal University of Rio Grande do Sul (Brazil) have been investigating the reuse of different agroindustrial wastes, including the incorporation of Pinhao and pecan nutshells into biocomposites using thermocompression, as part of the global drive to develop environmentally friendly material alternatives. They used their TA.XTplus Texture Analyser to perform tensile and flexural tests. Biocomposites containing pecan nutshells were found to present the lowest fracture stress and modulus values. However, the composites containing Pinhao nutshells had mechanical properties similar to the control sample. Find out more...
Research into uses of Vegetable Waste
Researchers from Tribhuvan University (Nepal) have been investigating the analysis of biodegradable films of starch from potato waste. The thriving use of non-biodegradable polymers has caused serious environmental problems and degradable polymers that are commonly prepared from renewable polymer sources have been paid more attention since the 1970s. In this study, starch was extracted from potato waste and peels to prepare biodegradable films using glycerol and sorbitol at various concentrations of dried starch, and the properties of films prepared with modification techniques analysed. They used their TA.XTplus Texture Analyser to measure the tensile strength and elongation of film samples, according to the standard method ASTM D882-02. Properties of modified starches were significantly different from non-treated starches. Read more
Scientists from the Federal University of Technology, Paraná (Brazil) have been researching cellulose nanofibres from cassava agro-industrial waste as reinforcement in PVA films. Cellulose nanofibres (CNF) have been applied in composite systems due to the abundance of raw material, excellent mechanical and thermal properties. In this work, cellulose nanofibres were prepared from agroindustrial waste and used in specified amounts in polyvinyl alcohol (PVA) composites. They used their TA.XTplus Texture Analyser to carry out tensile tests and an increase in the mechanical properties of PVA was observed with the addition of cellulose nanofibres. With 2.5% cellulose nanofibres in the PVA, the elastic module increased by approximately three times, with the addition of 10% cellulose nanofibres, a saturated system with poor mechanical properties was observed. Find out more...
Researchers from Fundación LEIA C.D.T, Spain, have been investigating lentil by-products as a source of protein for food packaging applications. There is an increasing need for biodegradable, environmentally friendly and functional food-packaging materials. In this regard, proteins obtained from agri-food industry by-products may become a promising and sustainable (less impact, valorisation) source of such materials. This work investigates the suitability of lentil protein-based films for food packaging applications. Lentil protein concentrate was extracted from lentil by-products using a procedure patented by SICA. Protein films containing different plasticisers were produced by casting after denaturation and adjusting the pH of the protein solution. The effect of plasticisers on solubility, moisture content and the mechanical and barrier properties was analysed.
They used their TA.XT2 Texture Analyser to perform tensile tests on film samples. Finally, migration tests were carried out. Plasticiser was found to have no effect on total soluble matter, although the moisture content increased in the case of glycerol. Films plasticised with sorbitol exhibited significantly lower water vapour and oxygen permeability and were also stronger and less flexible. Migration tests complied with current legislation in the case of isooctane but exceeded the legal limits for 95% ethanol. The results of this study confirmed that it is possible to obtain lentil protein films with suitable properties for food packaging applications from lentil by-products. These films may become a promising component of new biodegradable and functional food-packaging systems. Read more
Research into uses of Fish Waste
Researchers from Bhabha Atomic Research Centre, Mumbai, have been investigating the synthesis of biodegradable films using gamma irradiation from fish waste. Substantial waste is generated from fish processing industries causing pollution and health hazards. Hence, synthesising biodegradable film from myofibrillar protein dispersion of fish waste was attempted which may serve as “Wealth from Waste” – an eco-friendly initiative. Film dispersions were gamma-irradiated before casting and their physical properties were tested where film from non-irradiated dispersion served as control. They used their TA.HDplus to carry out tensile tests on film samples. The results showed the control had minimum tensile strength and maximum elongation at break whereas the irradiated samples had comparable values. Opacity with yellowness increased proportionally with dose. Find out more...
Applying the Texture Analyser to the Dental Industry in Compression, Flexure and Extrusion
According to Statista, the global dental market is projected to grow to around 37 billion dollars by 2021, and current indicators show that the market will keep moving forward, primarily driven by the implant sector. Its success is due to progress in the fields of medical technologies and implant materials. Texture Analysis has an important role in the dental industry; this article contains some examples of dental research in recent years.
A Texture Analyser is a very useful tool for the research and development associated with dental products and has the capability to perform both imitative and fundamental measurements. Dental product testing solutions from Stable Micro Systems include dental fixative adhesiveness, chewing gum hardness, stickiness and coating crispiness, toothpaste consistency and extrudability, and dental floss tensile strength, as well as many more.
Examples of how Dental Products can be Tested – Compression:
Scientists from Zhejiang University of Technology have been researching the fabrication and evaluation of dental fillers using customised moulds via 3D printing technology. In view of the high incidence and long-term treatment of dental caries, personalised dental fillers with long therapeutic action have broad application prospects in the dental clinic. The objective of this study was to fabricate and evaluate novel dental fillers using state-of-the-art 3D printing technology. To mimic the support from peripheral tooth tissue, the compression behaviour of the optimal dental filler was determined with customised compression moulds designed according to the printed mould, using their TA.XTplus Texture Analyser. The study confirmed that 3D printing was successful in designing and fabricating personalised dental fillers with high mechanical strength and “on-demand” drug release characteristics. Read more
Typical compression test on a Texture Analyser
Meanwhile, Mars Inc. have been fabricating animal jaws. They have recently released a patent, entitled ‘Animal dentistry apparatus and methods’. Chewable products are often used to improve the oral hygiene of animals as the chewing action can help to remove plaque. It is useful to understand the mechanical properties of these products as they can affect their performance in cleaning teeth; existing mechanical measurement techniques involve their compression with cylindrical probes. This patent addresses the shortcomings of in-vivo measurements with existing test methods for chewable products. They used their TA.HDplus Texture Analyser to perform tests with a mechanical jaw assembly. Read more
Mars develops a mechanical jaw device for their Texture Analyser
The Standard Test Method BS EN ISO 20126 is designed to test all aspects of manual toothbrushes, including bristle stiffness of the tufted area. The stiffness of toothbrush heads is a large factor in the choice made by the consumer during purchase. This property can be measured using a compression test – when compressing to a set distance, a larger force indicates stiffer bristles.
Examples of how Dental Products can be Tested – Flexure:
Scientists have been researching the mechanical properties of plain and reversed curve nickel-titanium archwires. In orthodontics, nickel-titanium wires are used for teeth alignment and levelling. The aims of this study were to investigate and compare the mechanical properties of wire samples, including unloading force, stiffness, springback and surface hardness, and they used their TA.XTplus Texture Analyser to perform these measurements. The reversed curve NiTi archwire had more unloading force and stiffness than plain NiTi archwire. For the correction of deep curve of Spee in orthodontic treatment, clinicians must be aware of the vertical force needed during intrusion of lower incisors or the wires should be used in the later levelling and aligning stage. Read more
Typical Flexure test on a Texture Analyser
Examples of how Dental Products can be Tested – Extrusion:
For products in tubes, the ability to squeeze the product out effectively is essential and is fundamental to its ease of removal from the packaging when required. If the substance is too dense, consumers will experience difficulty extracting it; if it is too fluid, the product could leak. In toothpaste manufacture, three characteristics of importance in consumer acceptance are absence of lumps or graininess, absence of air bubbles, and optimum consistency. All of these are greatly influenced by the manufacturing procedure and its control, as well as the selection of raw ingredients.
In terms of consistency, binders play a very important role. The purpose of the binder is to hold all of the ingredients of a paste together and to provide optimum consistency and texture. It is desirable that a toothpaste be easily squeezed out of the tube and break off cleanly when the desired amount has been extruded, but should not be so soft as to sink quickly into the brush.
The Sachet/Tube Extrusion Rig quantifies the force required to extrude the contents of toothpaste tubes and allows manufacturers to quantify the ease of removal and application of toothpaste as well as products such as ointments, creams and gels. The rig allows the positioning of the end of a sachet or tube vertically between two rollers, clamping the closed end with a grip at the top. The grip then pulls the sachet/tube upwards through the rollers, forcing the contents out. The higher the force recorded during this test, the more difficulty a consumer would experience in squeezing out the required amount.
This test was designed to provide product developers with a means to analyse changes in a product’s consistency throughout its shelf-life and adapt formulations accordingly, whilst also enabling manufacturers to assess the suitability of packaging material and its construction. Such a test at this stage of production could spell the difference between a successful and appealing product and one which will destroy the possibility of upgrading from sample sachet to long-term purchase of the high value larger volume personal care product. For manufacturers, failure at the last hurdle would bring disappointment and huge material losses.
Typical Sachet/Tube Extrusion test on a Texture Analyser
Texture Analysis in Research: How Texture Analysis is helping save our Planet
In a world that has woken up to the reality of climate change and other environmental matters, a large amount of research goes into developing eco-friendlier approaches to everyday objects and processes. Environmental concerns have become more important to consumers, leading many companies to design products around sustainability principles.
This can be focussed on reducing energy consumption in manufacturing processes, improving recyclability, using waste products or replacing materials with biodegradable alternatives. Texture Analysis plays an important role in ensuring standards are maintained in areas such as material mechanical properties and food texture. A large amount of research in this area occurs in an academic context; this blog post contains some examples of Texture Analysis in Research.
For example, putting waste products and industrial by products to use reduces the amount of matter that goes to landfill, and can reduce the total energy consumption of manufacturing processes.
In a recent study by researchers from the Institute of Agrochemistry and Food Technology, Spain, a material made from aquatic waste has been researched as a new method of cleaning up oil spills, and it also has applications in food packaging. They have been investigating PLA coatings to improve the performance of renewable adsorbent pads based on cellulosic aerogels from aquatic waste biomass. Lightweight, sustainable, hydrophobic pads were produced.
They used their TA.XTplus Texture Analyser to perform mechanical measurements, with compression strength increasing up to 10-fold with the incorporation of PLA. These materials presented a great potential as adsorbent pads for oil spill cleaning and food packaging applications. Read more
Over in Poland, scientists from Warsaw University of Life Sciences have been researching the production of innovative freeze-dried vegetable snacks with hydrocolloids in terms of technological process and carbon footprint calculation. Freeze-dried vegetable snacks were analysed in the form of a vegetable bar, which is residual waste from the production of frozen vegetables. Hydrocolloid bars were freeze-dried to create porous structure.
Two hydrocolloid systems were analysed: sodium alginate with calcium lactate and the mixture of locust bean gum with xanthan gum. They used their TA.HDplus Texture Analyser to measure the physical properties of obtained samples. and the carbon footprint for the production of each freeze-dried vegetables bar was calculated. The type of hydrocolloid was shown to have a significant impact on the on the physical properties and footprint of investigated snacks. Find out more
Another environmental problem that needs to be solved is the widespread overuse of single use plastics. Eco-friendly alternatives are being sought after by consumers and packaging manufacturers. In a study that put to use the waste from beer production, researchers from the University of Lisbon have been looking at a plastic with properties sufficient for use in plastic cups. They have been investigating product development with biopolymers made from brewers’ spent grain and carboxymethylcellulose, using a 3D food printer.
The combined use of recycling, reuse and biopolymers from various sources can be contributing factors for the reduction on environmental impact raised from the production, use and disposal of plastics. Brewers’ Spent Grain (BSG) is a by-product from beer production. In this context, the use of BSG to produce biomaterials can be an alternative for the destination of these residues from small and medium generators.
The main aim of this work was to develop a product with a BSG and CMC developed and characterised material, using a 3D printer. The material was developed, and physical proprieties was determined, followed by a 3D print of prototypes. They used their TA.XT2 Texture Analyser to perform three-point bend measurements on samples. The results showed that the materials prepared with BSG and CMC have high mechanical resistance and water resistance is enough to use in disposable cups. Find out more
In India, researchers have been investigating edible, biodegradable cutlery, reducing the disposal need for one large application of single use plastics. Scientists from Kongu Engineering College have been researching the optimisation of composition for the preparation of edible cutlery using Response Surface Methodology (RSM).
The objective of this study was to prepare nutritious edible cutlery using composite flour such as wheat flour, pearl millet and barnyard millet and optimise the composition based on water absorption characteristics at various temperatures under RSM. Levels of independent variables such as wheat flour, pearl millet and barnyard millet flour were varied.
They used their TA.XTplus Texture Analyser to perform Textural Profile Analysis on both raw and water-soaked samples. The optimum composition was found to be 50.12 % wheat flour, 26.18 % barnyard and 0% of pearl millet flour. The optimised sample had the nutritional value of 83.68 g/100g of carbohydrate, 2.36 g/100g of total fat and 5.67 g/100g of protein. It was found to biodegrade within 5 days. Read more
The reduction of energy consumption in any industry saves manufacturers money along with a lower impact on the environment. In the food industry, this can help contribute to a worldwide effort to strive for more sustainable food production. Over in Spain, researchers from the University of Murcia have been investigating the artificial light impact on the physical and nutritional quality of lettuce plants with an aim of looking into food production under sustainable conditions.
Recently, LEDs are being used extensively as a supplementary light source in indoor agriculture due to the economical and physiological advantages that this artificial illumination offers compared to traditional fluorescence illumination. In this work, two commercially important lettuce varieties were used to study the impact of LEDs (white and red–blue lights) and fluorescent illumination on their quality and health properties.
They used their TA.XTplus Texture Analyser along with a Kramer Shear Cell to measure leaf texture. They concluded that although several horticultural studies have been conducted to establish the effectiveness of LEDs in lettuce growth, additional investigations are necessary to determine the optimal conditions for the use of LEDs to promote lettuce production and the accumulation of beneficial components, such as vitamins, minerals, fibre and antioxidant compounds. Read more
In an effort to reduce the use of non-eco-friendly chemicals, scientists from the University of the Basque Country have been researching removable biobased waterborne pressure-sensitive adhesives (PSAs) containing mixtures of isosorbide methacrylate monomers. Growing environmental concerns are enforcing sustainable recycling processes for glass substrates, especially bottles, where a fast cleaning and minimisation of the use of solvents is desired.
In this process, labels and adhesives are mostly removed by the addition of harsh reagents, alkaline solutions, or high temperature, increasing economic costs and harming the environment. In this study, high performance and biobased waterborne pressure-sensitive adhesives with fast removability in water have been developed using small percentages of isosorbide (derived from glucose)-based methacrylate monomers.
They used their TA.HDplus Texture Analyser to perform peel, loop tack and probe tack tests. Formulations containing 2-octyl acrylate and isobornyl methacrylate and small amounts (1 wt %) of these monomers not only yield stronger adhesive fibrils, but also promote a removability in water 6× faster than that of nonisosorbide-based counterparts. This waterborne isosorbide containing PSAs represents an alternative to current PSA formulations toward more sustainable glass recycling and reusing processes. Read more
The fight against climate change will take a global effort from manufacturers and consumers, as well as global leaders and scientists. Texture Analysis has its part to play in this fight, ensuring the products we use every day are eco-friendly without a quality compromise.
Texture Analysis in Research: Latest Packaging Innovations
Researchers from the Indian Institute of Food Processing Technology have been investigating 3D printing of grinding and milling fractions of rice husk. With the aim of sustainability approaches and production of designer 3D food packages, this study examined the effect of printability of rice husk fractions of different size reduction methods. Extrusion tests were performed for both the rice husk fractions, and 3D printing process parameters were optimised for the ‘box’ shaped 3D model. Rheological behaviour and physical characteristics were analysed for all the material supplies.
They used their TA.HDplus Texture Analyser to measure the mechanical strength of the material supply and the effect of the addition of hydrocolloids. The study successfully demonstrated the conversion of non-printable rice husk into a printable form by the addition of guar gum into the milled fraction, which can be further utilised in food packaging, reducing the dependency on non-degradable petroleum-based plastics. Find out more...
Development of films
Scientists from Bhabha Atomic Research Centre have been researching the development of active / intelligent food packaging film containing Amaranthus leaf extract for shelf life extension of chicken and fish during chilled storage. There is a great demand in the food industry for intelligent packaging to evaluate real-time freshness of perishable food items such as meat and fish. Lately, several studies have reported the potential of natural pH sensing dyes for application in intelligent food packaging systems. However, the use of betalains extracted from Amaranthus leaves as a pH indicator dye has not yet been studied.
The aim of this study was to determine the bioactivity of Amaranthus leaf extract and to use it in development of an active and intelligent packaging film for shelf life extension of perishable food commodities like fish and meat. They used their TA.HDplus Texture Analyser to perform tensile tests on film samples. When applied to preservation of chilled fish and chicken, the films were active as they delayed microbial growth and minimised oxidative rancidity. Samples packed in neat films had a shelf life of 3 days while those in active films spoiled after 12 days. The film also showed visible colour change from red to yellow on spoilage. Read more
At the Federal University of Rio Grande, researchers have been researching chia seeds to develop new biodegradable polymers for food packaging, focussing on properties and biodegradability. Chia seeds are a promising raw material for the development of biodegradable and edible polymers due to their composition and properties. This study aimed to evaluate the effects of drying process of chia mucilage (oven and freeze‐drying) and the incorporation of chia oil in films for food packaging. The films were formed by casting using chia mucilage and glycerol. The polymers developed were evaluated by physicochemical properties, microstructure, thermal properties, and biodegradation.
They used their TA.XTplus Texture Analyser to measure tensile properties. The drying process of mucilage and oil incorporation in films affected mainly mechanical and colour properties. Freeze‐dried mucilage resulted in superior mechanical performance. Differences were caused by the effect of drying process in the molecular structure of chia mucilage and the incorporation of oil among the polymer chains. Chia mucilage films were completely soluble in water and biodegraded in a short time in soil. These films are promising biodegradable polymers for the development of eco‐friendly food packaging and edible sachets for small pre‐measured portions, preventing environment pollution and facilitating product consumption. Find out more...
Researchers from the Federal University of Rio Grande have been investigating hybrid starch / silica films with improved mechanical properties. Environmental concern has increased the research in the development of biodegradable packaging. Although there are many reports about starch films, their physicochemical properties need to be improved, and the introduction of an inorganic compound is an alternative to be applied. However, there are few reports about the development of biodegradable hybrid organic–inorganic films for food packaging. Therefore, the preparation of biodegradable films was proposed by using sol–gel and casting techniques, based on starch and glycerol as plasticisers, with the incorporation of an alkoxide precursor containing silicon, TEOS (tetraethyl orthosilicate) in different concentrations.
Morphological, thermal, optical, and mechanical properties, water solubility, swelling, and water vapour permeability were evaluated. They used their TA.XT2 Texture analyser to perform tensile measurements. The addition of TEOS was more efficient when it underwent pre-hydrolysis before incorporation into the film-forming solution, significantly interfering with the results of mechanical, optical, and barrier properties. The silica phase was uniformly incorporated into the polymer, presenting micrometric domains. The hybrid films produced have satisfactory properties for application as biodegradable packaging. Find out more...
Meanwhile at the University of Science, Malaysia, scientists have been researching the properties of hemicellulose based carboxymethyl cellulose film as a potential green packaging. Films were fabricated by incorporating hemicellulose in the range 0 to 80 wt%. They used their TA.XTplus Texture Analyser to perform tensile tests on film samples. 60 wt% of hemicellulose was identified as the optimum loading into carboxymethyl cellulose as a potential material for green packaging applications. Further the research aimed to develop the film structure by incorporating functional materials for future intended applications such as electrically conductive and photocatalytic thin films. Find out more...
Scientists from Laval University (Quebec) have been investigating divergicin M35-chitosan film, and its development and characterisation. Chitosan films loaded with bacteriocin were examined by FTIR spectroscopy, tested for colour, puncture strength, water vapour permeability, and as antimicrobials of Listeria innocua HPB13. They used their TA.XT2 Texture Analyser to perform puncture tests. Divergicin M35, a bacteriocin produced by Carnobacterium divergens, was incorporated into films made with chitosan of molecular mass 2 kDa, 20 kDa, or 100 kDa and de-acetylated either 87% or 95%. Only 100 kDa chitosan yielded films that could be peeled and handled easily. The higher degree of de-acetylation increased the total colour factor (ΔE) of bacteriocin-loaded films, their permeability, and puncture strength.
Incorporation of divergicin M35 into the films increased amide I peak intensity but otherwise did not induce significant structural change. The FTIR spectra of divergicin M35 shed from the films did not differ from those of the original free bacteriocin, except in overall peak intensity. The release of active divergicin M35 from the film was faster into the buffer than into tryptic soy broth and peaked at 10–12 h in both cases. Chitosan 95% de-acetylated and loaded with divergicin M35 was the most active, producing a six-log drop in Listeria innocua HPB13 viable count within 24 h. These results suggest that the biocompatible and biodegradable films developed here have the potential for application as antimicrobials of Listeria spp. in foods, especially ready-to-eat, minimally processed products. Find out more...
And at the Federal University of Rio Grande, researchers have been investigating biodegradable and active-intelligent films based on methylcellulose and jambolão skin extract for food packaging. Natural and environmentally friendly molecules like these are in high demand in the development of active and intelligent food packaging, to decrease food deterioration and indicate the product’s freshness, while preventing pollution. Jambolão (Syzygium cumini) is rich in anthocyanins, known by their antioxidant properties and colour changing in different pH environments.
In the present study, active and pH-sensitive films were produced by the incorporation of jambolão skins extract in methylcellulose films. Packaging related properties, crystallinity, contact angles, microstructure and thermal properties were determined to identify the effects of different concentrations of jambolão skin extract. They used their TA.XTplus Texture Analyser to perform tensile measurements on film samples. The films were found to offer the combined benefits to increase food shelf life and indicate product freshness, at the same time decreasing contamination. Potential applications include meat and aquatic products, where lipid oxidation occurs, and the pH modification of the food is associated with spoilage. Find out more...
Other packaging forms
Researchers from the Polytechnic University of Cartagena (Spain) have been investigating active cardboard boxes with smart internal lining based on encapsulated essential oils for enhancing the shelf life of fresh mandarins. Mandarins are usually sold in bulk and refrigerated in open cardboard boxes with a relatively short shelf-life (12–15 days) due to physiological and pathological disorders. The influence of a controlled release of essential oils from an active packaging was studied on the mandarin quality stability, comparing different sized cardboard trays and boxes, either non-active or active, at the pilot plant scale. They used their TA.XTplus Texture Analyser to perform penetration tests on whole fruits. The selected package was then further validated at the industrial scale.
Among package types, the active large box better maintained the mandarin quality, extending the shelf life from two weeks (non-active large box) to three weeks at room temperature. Particularly, the active large box highly controlled microbial growth, reduced weight losses, reduced acidity, and increased soluble solids (highly appreciated in sensory analyses), while it minimised colour and controlled firmness changes after three weeks. These trends were also observed during the validation experiment, extending the shelf life (based on sensory quality) from 14 to at least 21 days. In conclusion, the mandarin’s shelf life with this active cardboard box format was extended more than one week in refrigerated storage. Read more
Researchers from the University of Helsinki have been investigating active food packaging through controlled in situ production and release of hexanal. Transportation and storage of vegetables and fruits, including berries, is increasing to meet growing consumer demand for fresh foods. Ripening and softening of plant tissues may be slowed down by hexanal, a safe volatile compound that also has antimicrobial properties. Thus hexanal could be applied during the food distribution chain to slow down the spoilage of plant-based products and reduce food waste. Nonetheless, due to the rapid evaporation of hexanal, a constant supply is needed.
Their aim was to develop a concept to incorporate food-grade sunflower oil in a polysaccharide aerogel matrix for controlled in situ production and release of hexanal. They compared enzyme- and light-catalysed lipid oxidation reactions, determined the release of hexanal at different conditions, and performed storage stability tests of blueberries and cherry tomatoes. They used their TA.XT2i Texture Analyser to perform compression tests. The lipid-loaded aerogels assessed here are a potential novel delivery matrix for controlled hexanal formation to extend the shelf life of plant-based products. Find out more...
To review the typical types of tests used in the packaging industry for physical property measurement visit our Packaging Product testing page.
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Latest Texture Analysis in Research: Vegetables
Is there a best technique to cook vegetables? A study carried out at the University of Brazil about physical and sensory aspects to stimulate their consumption has attempted to answer this.
Consumers are becoming more health-conscious and have less time to prepare meals. They are often confused about which time and cooking method are adequate to preserve nutrients in vegetables. All cooking techniques cause changes in the nutrient content and the taste of a vegetable. The objective of this study was to determine the best cooking method for different vegetables using sensory evaluation and instrumental analysis of texture and colour. The chosen vegetables for this study were broccoli, carrot and Brazilian zucchini because they are among the most consumed vegetables in Brazil. The cooking methods were boiling, steaming, cooking in the combined oven, microwave, and steaming in the microwave.
They used their TA.XTplus Texture Analyser to evaluate vegetables for texture. In general, no significant differences were found by the panellists between intermediate cooking and more cooked points, allowing the definition of ideal time of cooking according to the one that best preserves vegetable nutrients. For global acceptance, the preferred cooking method was boiling for broccoli, steaming in the microwave for zucchini, and steaming or steaming in the microwave for carrot. For all the three vegetables, microwave cooking had the worst results regarding global acceptance. The instrumental analysis of texture and colour showed similar results to the acceptability variables. Find out more...
Researchers from the University of Arkansas have been investigating the comparison of instrumental methods for measuring seed hardness of food grade soybeans. Breeding specialty soybeans for the soyfood market requires proper methodology in evaluation of seed quality attributes. In this study, efficient methods that could be potentially used for testing soybean seed hardness were developed by examining different instruments and seed parameters. Seed hardness is an important factor in determining soybean suitability for natto production.
This study used two Texture Analysers equipped with five different probes to test hardness of five soybean genotypes with different seed size. The methodologies for testing the seed texture of soybean have been established in this publication, which can help regulate the seed hardness testing for commercial production and provide consistent hardness references for natto breeding programmes and the seed industry. Read more
Scientists from Jiangnan University have been researching the application of sensory and instrumental techniques to evaluate the texture of French fries. The aim of this study was to explore the relationship between instrumental and sensory data and to select the type of probes suitable for determining the texture of French fries. They used their TA.XTplus Texture Analyser to measure texture parameters of samples at 50°C. Ten commercial French fries were assessed using different probe types and perceived sensations through descriptive analysis. The eight sensory attributes developed by trained panellists were found to distinguish samples well.
The result of instrumental data analysis revealed that the variation coefficient of three‐point bending was the largest, which indicated that the measurement accuracy was lower. The compression test showed significant correlation with most of the sensory attributes, while the cutting test with Volodkevich Bite Jaws did not correlate with all sensory attributes. Among these instrumental methods, compression, blade with guillotine probe, and puncture test were recommended for texture analysis of French fries. These results will provide a time‐saving and efficient method for determining the texture of French fries. Find out more...
A patent has recently been released by Conagra Foods RDM, entitled ‘Shelf Stable Fried Product and Process for Creating the Same’. The aesthetic properties of shelf stable fried food products are a contributor to consumer appeal. Previous processes for creating shelf stable fried food products resulted in a less desirable shelf stable food product. In this patent, the fried product contains a whole cut of vegetable or fruit, as well as a crispy and crunchy texture and a resistance to staling. The shelf stable fried product can be packaged to facilitate on-the-go snacking where consumers are not required to cook, thaw, heat or otherwise further prepare the product prior to consuming the product from the package. They used their TA.XTplus Texture Analyser to perform cutting tests with a Fracture Wedge Set. Find out more...
Researchers from the University of Reunion Island have been investigating fruit density as a reliable indicator of sensory quality for mango. There is constant demand from the fresh fruit sector for reliable, non-destructive indicators to better predict the sensory quality of fruits. The aim of this study was to evaluate the relevance of density to predict mango sensory quality at the ripening stage. Models were built from density and the day of maturation to predict physicochemical indicators of sensory quality. They used their TA.XT2 Texture Analyser to measure pulp firmness. Mangoes with a higher density were found to have a significantly higher intensity of sweetness, mango aroma, and lower intensity of firmness than mangoes with the lower density, whatever the origin. Read more
And finally, scientists from University Putra Malaysia have been investigating the characteristics of powders produced from different parts of sweet potato. Sweet potato is a staple food in developing countries because of its short growing duration. Different parts of the sweet potato plant may offer various benefits, but there is a lack of understanding on the properties to link with its potential applications.
The objective of this study was to determine the characteristics of powders produced from different parts of sweet potato including stem, leaves, tuber and skin. They used their TA.XTplus Texture Analyser along with a Powder Flow Analyser to perform cohesion tests, Powder Flow Speed Dependency tests and caking tests. The study showed that the powder of sweet potato stem, leaves, tuber and skin are categorised as free and stable powders and also prone to cake. Find out more...
• Discover the typical types of tests used in the fruit and vegetable industry for texture measurement
• Request our articles that give an overview of all of the methods available for fruit and vegetable product testing
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• View published references on research using our instruments for vegetable product testing
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• See how Fruit & Vegetable Industry Leaders use Texture Analysis to get ahead of their competition
Texture Analysis in Research: Medical & Surgical Advances
Researchers from the University of Indonesia have been investigating a TUR-P phantom for resident surgical training – a food-based design as a human mimicking model of the prostate. The novel model aimed to be similar to the human prostate in terms of its texture profile, sensation upon resection, and anatomical hallmarks for resident transurethral resection of the prostate training. Ten phantom designs were proposed, using broadly available ingredients and a homemade protocol. They used their TA.XT2i Texture Analyser to measure the samples’ texture profile. The study successfully developed a cost-effective model from a food-based design. Read more
Meanwhile, a novel simulation model for transabdominal preperitoneal (TAPP) inguinal hernia repair is being investigated by researchers from Pirogov Russian National Research Medical University. TAPP inguinal hernia repair requires the surgeon to have good manual skills in laparoscopic surgery, as well as an understanding of the laparoscopic features of the groin anatomy. This is why TAPP is considered a more difficult surgical procedure compared to open techniques. A realistic training model for TAPP inguinal hernia repair would enhance surgeons’ skills before they enter into the operation room.
The aim of this study was to create a realistic, inexpensive, and easily reproducible model for laparoscopic TAPP inguinal hernia repair and to assess its effectiveness. The applied TAPP inguinal hernia repair training simulator consists of a laparoscopic box and an inguinal region model placed in it. The model of the groin area is made of the porcine stomach and assembling materials. They used their TA.XTplus Texture Analyser to perform uniaxial tensile and T-peel tests to compare the mechanical properties of the porcine stomach and the human cadaver peritoneum. The study was successful in creating a model for TAPP inguinal hernia repair training made of inexpensive synthetic and biological materials similar to the human tissue. The model is easy to reproduce and can be used in the training programs of surgical residents. Read more
Cardiotoxicity is a common reason for drug withdrawal, but it is a difficult effect to measure. Animal experiments in this field are unethical and poor predictors of human toxicity, so a human cardiac tissue model is a good solution. Scientists from Tampere University have been researching the direct measurement of contraction force in a human cardiac tissue model using a piezoelectric cantilever sensor technique. To question the cardiotoxicity of a drug, a model such as this is used to measure the contraction force of cardiac muscle cells. They used their TA.XTplus Texture Analyser to measure the voltage vs force sensitivity of cantilever sensors. Development of the measurement method allowed very low forces to be determined, such as those that appear in biological small scale systems. Read more
Meanwhile in the field of surgical progress, scientists from the National Institute for Materials Science, Japan, have been investigating underwater adhesive microparticle dressings composed of hydrophobically-modified Alaska Pollock gelatine for gastrointestinal tract wound healing. The goal of this study was to develop wound dressings with strong tissue-adhesive properties to living tissues for promoting wound healing after endoscopic submucosal dissection (ESD). Monodisperse microparticles composed of hydrophobically-modified Alaska pollock gelatine were prepared by self-assembly of gelatine in water-ethanol mixed solvents and thermal crosslinking. They used their TA.XT2i Texture Analyser to measure the adhesion strength and adhesion energy of samples according to ASTM F-2258-05. Optimal hydrophobic modification drastically improved underwater stability of microparticles. The in-vivo studies were performed to evaluate the ability of this colloidal wound dressing to suppress fibrosis. This new biomaterial has enormous potential to promote wound healing after ESD. Read more
Scientists from the University of Texas at Austin have been researching polysaccharide-based films for the prevention of unwanted postoperative adhesions at biological interfaces. Postoperative adhesions protect, repair, and supply nutrients to injured tissues; however, such adhesions often remain permanent and complicate otherwise successful surgeries by tethering tissues together that are normally separated. An ideal adhesion barrier should not only effectively prevent unwanted adhesions but should be easy to use. However, those that are currently available have inconsistent efficacy and are difficult to handle or to apply. A robust hydrogel film composed of alginate and a photo-crosslinkable hyaluronic acid derivative represents a solution to this problem.
In this study, a sacrificial porogen (urea) was used in the film manufacture process to impart macropores that yield films that are more malleable and tougher than equivalent films produced without the sacrificial porogen. They used their TA.XTplus Texture Analyser to measure the puncture resistance of samples. The robust mechanical behaviour of these films directly facilitated handling characteristics of the barrier film. In a rat peritoneal abrasion model for adhesion formation, the polysaccharide films successfully prevented adhesions with statistical equivalence to the leading anti-adhesion technology on the market, Seprafilm®. Read more
Texture analysis continues to be used in many other areas of the medical world. Many patients suffer from traumatic peripheral nerve injuries every year. A considerable proportion of these patients are young people who constitute the main labour force of society. Nerve injuries cause dysfunction in the extremities and affect work and living abilities, which brings society a huge burden. The functional recovery of peripheral nerve injuries is associated with many factors, including the time interval between the injury and repair surgery. Researchers from the AJA University of Medical Sciences, Tehran, have been investigating the regenerative capacities of a chitosan-nanoselenium conduit on transected sciatic nerves in diabetic rats. They used their TA.XTplus Texture Analyser to perform tensile tests on regenerated nerves. Chitosan-nanoselenium conduits were found to result in accelerated functional recovery. Read more
Also in the field of eyes, researchers from the University of Iceland have been investigating in vitro and ex vivo evaluation of nepafenac-based cyclodextrin microparticles for treatment of eye inflammation. Inflammation of the eye and surrounding tissues is among the ocular pathologies with the highest incidence in ophthalmology, and when deprived of the appropriate treatment, can lead to visual loss. The aim of this study was to design and evaluate novel cyclodextrin (CD)-based aggregate formulations to efficiently deliver nepafenac topically to the eye structure, to treat inflammation and increase nepafenac levels in the posterior segment, thus attenuating the response of inflammatory mediators. They used their TA.XTplus Texture Analyser to measure mucoadhesion strength of eye drop samples on bovine corneas. The optimised formulations represented an opportunity for topical instillation of drugs to the posterior segment of the eye. Read more
Scientists from Sher-e-Kashmir University of Agricultural Sciences and Technology have been researching nutrient selection and optimisation to formulate a nutrient bar stable on storage and specific to women at risk of osteoporosis. Osteoporosis is a silent but progressive disease affecting not only the bone mineral density but also the quality of one’s life, while greatly increasing fracture risk. The current study was carried out with the objective of preparing a multi-nutrient supplement by selecting and characterising different food ingredients preferably from plant origin at optimised levels, to analyse their nutritional suitability and storage stability in the form of nutrition bars for improving the bone health of post-menopausal women. They used their TA.HDi Texture Analyser to perform textural profile analysis on samples. It was concluded that functional foods with healthy nutrients prepared for women at risk of osteoporosis not only aid in their bone health but are also commercially viable. Read more
Alternatively, request our articles that give an overview of all of these methods for pharmaceutical and medical product testing.
Texture analysis in Research: Formulating for an ageing population
Scientists from Poznań University of Life Sciences have been evaluating the mechanical and sensory characterstics of selected foodstuffs for senior citizens. The population of Poland is one of the fastest ageing communities in Europe. Consequently, it is necessary to adapt the daily diet to these consumers’ requirements. The potential producers of food for senior citizens must allow for elderly people’s possibilities to consume meals (the structural aspect) and their nutritional needs.
The aim of the study was to perform an instrumental analysis of the mechanical properties and sensory evaluation of selected foodstuffs for senior citizens. They used their TA.XT2i Texture Analyser to perform shear tests and penetration tests of selected samples. The results of the instrumental and sensory tests showed that the products developed for senior citizens had desirable structural characteristics, which are important for their consumption. As the issue of food for senior citizens is important for consumers all over Europe, it is necessary to consider the taste preferences of consumers inhabiting a particular geographical region (traditional flavours) before such foodstuffs are offered on the market. Read more
Meanwhile, scientists from the Institute of Food Science, Technology and Nutrition, Madrid, have been researching oral processing of six solid foods, using both objective and subjective characterisation. Research into oral processing is becoming increasingly important with an ageing world population. Consequently, a new strategy is needed for the instrumental assessment of texture perception, with capability to measure dynamic bolus formation. This study chose banana, apple, carrot, cured ham, peanut and potato chips as solid foods with very different textures. They used their TA.HDplus to perform tests using the Miniature Kramer Shear Cell to assess the mechanical properties of these foods and of their bolus counterparts to determine how foods’ mechanical properties change during dynamic oral processing. Read more
Researchers from the University of Hertfordshire have been investigating the swallowing characteristics of thickeners, jellies and yoghurt observed using an in vitro model. Drinks and foods may be thickened to improve swallowing safety for dysphagia patients, but the resultant consistencies are not always palatable. Characterising alternative appetising foods is an important task. The study aimed to characterise the in vitro swallowing behaviour of specifically formulated thickened dysphagia fluids containing xanthan gum and/or starch with standard jellies and yoghurt using a validated mechanical model, the “Cambridge Throat”. They used their TA.XTplus Texture Analyser to evaluate the textural characteristics of samples. The in vitro results showed correlation with published in vivo data though the limitations of applying the in vitro swallowing test for dysphagia studies were noted. These findings contribute useful information for designing new thickening agents and selecting alternative and palatable safe-to-swallow foods. Read more
The Public University of Navarre have been investigating the methodology for design of texture-modified dishes for dysphagic patients. This study presents the design of suitable ready-to-eat dishes for dysphagic people. The methodology developed is of great interest to the industry of ready-to-eat dishes. Instrumental and sensory texture analyses were useful in studying thermostability. They used their TA.XT2i Texture Analyser to perform back extrusion tests. The methodology was found to be appropriate for developing suitable dishes, sensorially accepted by dysphagic people, thermostable for seven days in refrigerated storage and ready-to-eat. Read more
At Zhejiang Gongshang University, scientists have been performing cohesiveness visual evaluation of thickened fluids. Cohesiveness is recognised as an important property of food for medical management of individuals who suffer from swallowing difficulty (known as dysphagia). However, while the term cohesiveness is commonly used for the description of such products, its sensory nature and instrumental assessment remain a big challenge.
Therefore, the aim of this work was to compare and correlate the rheological parameters of thickened fluids with the perceived cohesiveness obtained from the sensory analysis by visual perception. They used their TA.XTplus to measure the cohesiveness of fluid by assessing syringe extrusion flow behaviour, measuring the droplet aspect ratio when extruded at a constant speed, just before the fluid breaks. This technique was highly correlated with the perceived cohesiveness from the visual perception and could be used as a standardised methodology of evaluating cohesiveness of semi-solid and liquid materials for industrial purposes. Read more
Request our article Designing foods with specific health claims for an ageing population which gives an overview of suitable methods for assessing this type of food formulation.
Tribology testing continues on the Texture Analyser
Scientists from the University of Queensland have been investigating tribology and its growing use in the study of food oral processing and sensory perception. Studies on “soft-tribology” have emerged to provide knowledge and tools to predict oral behaviour and assess the performance of foods and beverages. This study has shown that there is a now a comprehensive set of fundamental literature, mainly based on soft contacts in the Mini-traction machine with rolling ball on disk configuration, which provides a baseline for interpreting tribological data from complex food systems.
Tribology-sensory relationships do currently exist. However, they are restricted to the specific formulations and tribological configuration used, and cannot usually be applied more broadly. A modified TA.XT2 Texture Analyser with a ‘plate on three balls’ configuration has been used to measure friction in an oral processing context. With a careful and rigorous formulation/experimental design, the researchers envisage tribological tools to provide insights into the sensory perception of foods in combination with other in vitro techniques such as rheology, particle sizing or characterisation of surface interactions. Read more
Within this field of interest, researchers from Zhejiang Gongshang University have been investigating the oral tribology of saliva-tea compound mixtures, correlating sweet aftertaste perception and friction coefficient. Sweet aftertaste (Huigan) is a sensation perceived after drinking tea, and lasts in the mouth and throat, leading to salivation for an extended period of time.
The study aimed to reveal the underpinning mechanisms of Huigan and its influencing factors. A tribology approach was applied in conjunction with sensory analysis and other physiology assessments. They used their TA.XTplus Texture Analyser to manufacture an in-house tribometer setup for lubrication studies. The Huigan intensity perceived by the sensitive group was found to be highly correlated with the friction coefficient measured, especially at sliding speeds lower than 0.5 mm/s. Read more
Scientists from Wageningen University & Research have been investigating the friction behaviour of intact soft solid foods and food boli. The structure of soft solid foods changes dynamically throughout its consumption; food is reduced in size, mixed with saliva and enzymes, and a cohesive mass is formed. During this process, the mechanical properties of food change, as does the perception.
In order to know how processing and composition of foods affect sensory perception, the dynamic changes in the rheological and tribological behaviour of foods have to be studied. They used their TA.XTplus Texture Analyser to perform compression tests on soft solid food gels and sausages. The decrease in friction by saliva was found to be boli particle dependent. Read more
Whilst not performing tribology tests, scientists from Wageningen University have also been investigating strategies to compensate for undesired gritty sensations in foods. The study aimed to investigate whether the addition of macroscopic particles or fat to quark can be used to compensate for negative texture sensations such as grittiness by either psychological or physical mechanisms. They used their TA.XTplus Texture Analyser to characterise the mechanical properties of granola and peach gel pieces using a cutting test.
The addition of crunchy granola pieces or fat was a useful strategy to shift and increase dominance of positive and liked attributes, leading to an increase of overall liking, although negative sensations such as grittiness caused by microparticles were still perceived. This approach could be used to compensate for undesired texture sensations in different types of foods, such as high protein foods. Read more
More recently, Jianshe Chen and his colleagues have continued to make progress using the Texture Analyser for tribology and have published the following paper: ‘A new design of soft texture analyser tribometer (STAT) for in vitro oral lubrication study’ which uses 3D printed components. Read more
The Packaging Research Revolution: Biodegradable Polymer Foams and Rubbers
A major focus of current research in both industrial and academic institutions is the development of suitable alternatives to single use plastics. This has been driven by the worldwide push for a cleaner environment, and both the manufacture and disposal of plastics are harmful in separate ways. Packaging is a large contributor to plastic production, particularly the single use sector. One method of reducing this production is to replace traditional polymers with biodegradable alternatives. A drawback of biodegradable plastics is their reduced strength and toughness. Mechanical properties are an important consideration when it comes to packaging, so their control is a crucial stage in the R&D process. Consequently, Stable Micro Systems feature heavily in publications from this field. The following are a selection of recent journal papers, specifically those focussing on polymer foams and rubbers.
Researchers from Ohio State University have been investigating the optimal mechanical properties of biodegradable natural rubber-toughened PHBV bioplastics intended for food packaging applications. The incorporation of natural rubber into PHBV through melt blending improves its flexibility and toughness but sacrifices tensile strength, due to low rubber modulus and insufficient compatibility between the two materials. These unbalanced mechanical properties restrict the use of this blend in packaging applications. The objective of this study was to optimise the mechanical properties of PHBV/natural rubber blends by using peroxide and coagent. They used their TA.XT2 Texture Analyser to measure the strength of seals in a tensile test. Optimal mechanical performance of natural rubber toughened PHBV bioplastic was obtained using a combination of testing techniques. Read more
Researchers from the Federal University of Rio Grande do Sul have been investigating biodegradable starch-based foams incorporated with grape stalks for food packaging. As part of the enormous drive to reduce the use of disposable plastics in packaging, this study looks into the use of naturally-sourced packaging options. They used their TA.XT2i Texture Analyser to perform flexural tests of the foams according to ASTM D 790-03. Foams completely biodegraded after 7 weeks, demonstrating that for the experimental conditions used, the interactions between the starch and grape stalks did not generate recalcitrant compounds or structural alterations that would impair foam degradation. Furthermore, the foams including grape stalks presented good properties in the applicability test, showing a promising application in the storage of foods with low moisture content. Read more
Researchers from the Federal University of Jequitinhonha and Mucuri Valleys have been investigating biodegradable trays based on cassava starch blended with agroindustrial residues. Biodegradable materials are an alternative to traditional synthetic polymer-based packaging materials. When they are discarded into the environment, they are easily degraded into simpler compounds that can be metabolised by bacteria, yeasts and fungi. Among biodegradable materials, materials derived from renewable resources (e.g., starch) have received increasing attention because they combine environmental and functional benefits. This study investigates how the fibrous agroindustrial residue concentration affects the properties of the biodegradable trays and compares these characteristics with the features of expanded polystyrene trays. They used their TA.XTplus Texture Analyser to perform tensile tests on tray samples. The study found that fibrous agroindustrial residues can potentially be employed to produce biodegradable trays, especially the combination of sugarcane bagasse and cornhusk. Read more
The Packaging Research Revolution: Biodegradable Polymer Films
The majority of countries worldwide are making an effort to reduce their mark on the planet, and cutting down on plastics is an obvious place to start because of the availability of alternatives, and due to the large amount of waste they leave behind. One of the largest sources of single use plastics is packaging. There is a large amount of academic and industrial research into this area. Stable Micro Systems equipment is a regular feature of publications due to the need for mechanical property analysis; one of the drawbacks of biodegradable polymers is their reduced structural integrity. Consequently, Texture Analysers are necessary to perform tests for both R&D and quality control, once the product has reached production. The following are a selection of recent publications into this interesting and important field, specifically those focussing on polymer films.
Scientists from the University Putra Malaysia have been researching tapioca starch films reinforced with microcrystalline cellulose for potential food packaging applications. This work was directed towards developing biodegradable films from a biopolymer that is sustainable and environmentally friendly, particularly tapioca starch. They used their TA.XTplus Texture Analyser to perform tensile tests on film samples. The ideal filler addition was found as a result of this study, resulting in the highest performance of films’ mechanical and barrier properties. Thermal properties were also improved. In conclusion, films produced in this study exhibited improved properties and have the potential to be used for food packaging applications. Read more
Researchers from the Federal University of Rio Grande have been investigating the use of different proteins to produce biodegradable films and blends. The synthesis of new biomaterials with optimised performance and properties is a constantly expanding area in food packaging technology. A significant advancement in this area has occurred with the synthesis of blends consisting of natural polymers from different origins. This class of material has aroused great interest among researchers in recent decades because it is a simple and practical alternative, resulting in materials with improved characteristics for application in packaging. The objective of this study was to develop, characterize and evaluate biodegradable films produced from different proteins and their blends. They used their TA.XTplus Texture Analyser to carry out tensile tests on film samples to give tensile strength and percentage elongation. One film formulation stood out by presenting good mechanical and thermal resistance along with complete biodegradability in less than 10 days, proving to be the most promising blend for the development of sustainable materials for food packaging. Read more
Scientists from the University of Santiago de Compostela have been researching environmentally friendly films containing bacterial cellulose, chitosan and polyvinyl alcohol, particularly the effect of water activity on barrier, mechanical and optical properties. The interest in developing new materials intended for food packaging based on bacterial cellulose has been growing in recent years. Flexible and transparent films from bacterial cellulose−chitosan−polyvinyl alcohol have shown excellent UV-barrier properties. However, this material interacts with ambient moisture modifying its water activity due to its hydrophilic nature. In this work, a study was carried out to evaluate the changes caused by the water activity. They used their TA.XTplus Texture Analyser to perform tensile tests on film samples. Results showed a plasticising effect of water molecules increasing the water vapour permeability of the samples, percentage of elongation and distance to burst. The increase of the water activity decreased the Young’s modulus and tensile strength. The values of the UV-barrier were maintained at the wide range of water activity. Consequently, water molecules do not affect the UV-barrier properties of the films. Read more
Researchers from Tezpur University have been investigating the valorisation of pumpkin seeds and peels into biodegradable packaging films. Pumpkin seeds and peels are waste generated from the pumpkin processing industry and having the potential to utilise for biodegradable film development. Such biodegradable films were developed with defatted pumpkin seeds and pumpkin peels. They used their TA.HDplus Texture Analyser to measure the tensile strength and elongation at break of films. The study showed that co-products of the pumpkin processing industry can successfully be used for developing biodegradable films. Find out more
Texture Analysis in Research: Meat & Meat Substitute Products
Researchers from the Institute of Food Science, Technology and Nutrition, Madrid, have been investigating ethyl cellulose and beeswax oleogels as fat replacers in meat products. The effect of storage over 28 days was evaluated by measuring physiochemical, mechanical and viscoelastic properties of both oleogels before and after storage.
They used their TA.XTplus Texture Analyser to perform penetration tests. Ethyl cellulose produced more deformable and cohesive gels with greater time- and temperature- stability than their beeswax counterparts which resulted in rigid and brittle gels. Their oxidative stability, mechanical and rheological properties were very stable during the chilled storage period, suggesting that both organogels could be stored up to 15 days prior to use without significant change in their composition or technological properties. Read more
Meanwhile, as interest for the development of food for ageing populations increases, scientists from Dalian Polytechnic University have been carrying out a feasibility study of hydrocolloid incorporated 3D printed pork as dysphagia food. The application of 3D printing technology in the food field is expected to contribute towards the design and development of innovative food products available for a wide market with diverse consumers’ needs and demands.
For instance, one of the most relevant applications remains on the production of customised 3D printed meals for people with chewing and swallowing difficulties, like dysphagia sufferers, for whom each mealtime may represent a risk of choking and aspiration, due to a problem with swallowing co-ordination or mechanical obstruction. They used their TA.XTplus Texture Analyser to perform forward extrusion tests on pork pastes to estimate the force required for extrusion during the printing process. Gum blend addition along with 3D printing was found to produce a lower density meat microstructure. Read more
At the University of Veterinary and Animal Sciences, Lahore, researchers have been investigating the meat quality and cooking characteristics in broilers influenced by winter transportation distance and crate density. Broiler welfare and meat quality are serious concerns for the poultry industry worldwide, and studies such as this are crucial in maintaining high welfare standards, which directly influence meat quality.
After being transported one of three known distances in one of three known crate densities, birds were slaughtered, and breast meat quality parameters including pH, colour, drip loss, shear force, marinade uptake and retention, cooking losses, and yield were determined. They used their TA.XTplus Texture Analyser to perform mechanical measurements on raw and marinated meat, using a Warner Bratzler blade for shear testing. It was found that an increase in transportation distance and low crating density during winter can negatively affect physical quality of meat with significant improvement in marination and cooking characteristics. Read more
Interest in the plant-based meat market is thriving globally with UBS predicting that sales could grow by more than 25% a year to $85 billion by 2030. Plant based meat is disrupting the animal meat industry. Its food products are made to replicate the properties of natural meat and work like meat substitutes. It is more sustainable and environmentally friendly than conventional meat products. Food products like Textured Vegetable Protein (TVP), Tofu, Quorn, Tempeh, and Seitan are made to simulate the appearance, flavour and texture of animal meat products.
Researchers from the Chinese Academy of Agriculture Sciences have been investigating the conversion of peanut protein biomass waste into ‘double green’ meat substitutes using a high moisture extrusion process in a multiscale method to explore a process for forming a meat-like fibrous structure. Converting peanut protein biomass waste into environmentally friendly meat substitutes by a high-moisture extrusion process can help solve both resource and waste problems and be “double green”.
A multiscale method combined with some emerging techniques such as atomic force microscopy-based infrared spectroscopy and X-ray microscopy was used to make the whole extrusion process visible to show the process of forming a meat-like fibrous structure using 2D and 3D perspectives. They used their TA.XT2 Texture Analyser to measure the lengthwise strength, crosswise strength and fibrous degree (the ratio between the two strengths) of samples. The study successfully described the different stages in the formation of a fibrous meat substitute. Read more
To review the typical types of tests used in the meat industry for texture measurement, visit our Meat and Fish Testing page
Alternatively, request our articles that gives an overview of all of these methods for meat and meat substitute testing
See how Meat Industry Leaders use Texture Analysis to get ahead of their competition
Research examples from the field of Cosmetics
Researchers from Avon Products, Inc. have been investigating technical approaches to select high‐performance instant skin smoothing formulations, looking at the correlation of in vitro and in vivo assessment methods.
Contractile films that smooth the surface of skin upon drying are popular among consumers due to their “instant” effect and perceivable smoothing benefits. The objective of this study was to correlate an in vitro measurement of contractile force with in vivo smoothing performance, enabling rapid screening of film‐forming technologies for high impact cosmetic results.
An in vitro method is introduced to measure drying stress of film‐containing formulations. The tested formulas have also been evaluated in a blinded clinical study, measuring their effect on under‐eye and Crow's Feet area smoothing through bioinstrumentation (3D PRIMOS imaging) and blinded expert grading of images.
To measure in vitro drying stresses, a tensile test method was adapted using a TA.XTplus Texture Analyser inside an environmental control box. The in vitro drying stress measurement was found to be repeatable and sensitive enough to detect differences between formulations with typical amounts of film‐forming agents. Significant correlation was found between the in vitro drying stress measurements and under‐eye smoothing measured by 3D imaging.
Expert grading confirmed that film formulas deliver perceivable smoothing in the under‐eye and Crow's Feet regions 15 minutes after application. Read more
Scientists from the University of Coimbra have been researching cream formulations with the aim of establishing a framework to screen and understand the product variability from factors that affect the quality features of cream formulations. Physiochemical measurements included Texture Profile Analysis using their TA.XTplus Texture Analyser along with stability studies.
This study revealed the potential of Quality by Design methodology in understanding product variability, recognising the most critical independent variables for the final product quality. This systematic approach in the pharmaceutical field will yield more robust products and processes, provisioning time and cost effective developments. Read more
Scientists from the University of Paris-Saclay have been researching the role of lipid composition in the sensory and physical properties of lipsticks. The perception of lipstick texture upon application is a key driver of consumer satisfaction. However, formulators may only rely on the absence of knowledge about the relationship between ingredients and product sensory properties. Lipsticks are made of a complex anhydrous mixture that contains about 80% lipids (oils, waxes, and butters). The goal of this work was thus to investigate the combined effect of multiple lipid ingredients on the sensory and physical properties of a cosmetic product such as lipstick.
The researchers first analysed a typical lipstick formula and its related ingredient categories. This allowed them to create a simplified yet realistic lipstick system. Based on this, they formulated 36 lipsticks varying in oil and butter composition according to three mixture designs. All products were evaluated by a panel of sensory experts — with a focus on the slipperiness and melting perception — and analysed using texture measurements on their TA.XTplus Texture Analyser.
The physical and sensory results both showed that oils had the strongest impact on the lipstick properties while the impact of butter was negligible. Moreover, the perceived slipperiness of lipsticks was closely related to the viscosity of the oil mixture present in the formula. Read more
Researchers from the Herminio Ometto Foundation, Brazil, have been investigating the assessment of an anti-ageing structured cosmetic formulation containing goji berry. Based on previous studies, it has been found that goji berry (GB), popularly known as a ‘miracle fruit’, has excellent antioxidant potential and can be used in the treatment of skin disorders associated with ageing.
This study aimed to incorporate GB into a structured cosmetic in order to optimise its penetration. Stability studies of the formulation, determination of the antioxidant activity of the extract and of the formulation, rheological measurements, SAXS, polarised light microscopy and bioadhesion analyses were performed. They used their TA.XTplus Texture Analyser to perform the bioadhesion measurements with porcine ear skin as a substrate. In vitro bioadhesion experiments revealed that these formulations exhibited skin adhesion strength statistically similar to commercial anti-ageing formulation.
These results suggest that this formulation has excellent potential to be used as a topical treatment for ageing. Read more
Researchers from Pondicherry University have been investigating the photoprotective effect of nanomelanin-seaweed concentrate in formulated cosmetic creams, with improved antioxidant and wound healing properties.
This study aimed to formulate a cream by incorporating melanin from marine sponge associated bacteria and seaweed concentrate. They used their TA.XTplus Texture Analyser to perform back extrusion of cream samples. Texture analysis of newly formulated cream showed similar results with that of control cream in terms of firmness, cohesiveness, index of viscosity and consistency.
This study was the first report on photoprotective cream formulation using melanin and seaweed concentrate, which improved antioxidant and wound healing properties. The antimicrobial effect of the formulated natural cream could reduce the emergence of drug resistant bacteria and side effects of synthetic creams. Read more
To review the typical types of tests used in the cosmetics industry for texture measurement visit our Cosmetics & Skincare Testing page. Alternatively, request our articles that gives an overview of all of these methods for cosmetics testing.
Research in the Confectionery industry
The food industry is flourishing at a very high rate all across the globe and might serve as a major driver for the confectionery ingredients market. Confectionery ingredients provide stability, texture, and various other properties, and therefore, can be used to prepare a variety of food products. More than 70% of consumers prefer the use of products that contain natural ingredients and therefore chose the products that claim to have no artificial ingredients. The trend for the use of clean-label products is rising due to the increase in health awareness among the consumers, and therefore, the manufacturers of confectionery products are attempting to make use of ingredients to develop innovative products that have low-fat content, low sugar content, etc. The development of such food products might attract health-conscious consumers, and thus, there might be an increase in the confectionery ingredients market.
Scientists from the University of Birmingham have been researching the development of fat-reduced chocolate by using water-in-cocoa butter emulsions. The production of low-fat chocolate represents a challenge in the food industry as fat provides the chocolate main characteristics. In this work, water-in-cocoa butter emulsions were used to partially replace fat. First, the emulsion was optimised in terms of formulation and process parameters to achieve the maximum fat replacement and the required properties in terms of droplet size, free water and thermal behaviour. Afterwards, the emulsion was mixed with cocoa powder, icing sugar and milk powder to make the full chocolate. The effects of the mixing temperature and stirring rate were investigated. They used their TA.XTplus Texture Analyser to measure the hardness of samples in terms of three point bend breaking strength. It was demonstrated that with this approach it is possible to develop a low-calorie chocolate, characterised by 40% less fat, with properties close to the full fat equivalent. Read more
Meanwhile, there are technical issues that other manufacturers are attempting to resolve: biodegradability and 3D printing.
Researchers from Islamic Azad University have been investigating the production of bio-chewing gum based on the biopolymer Saqqez, with emphasis on its biodegradability and textural properties. Commercially, chewing gum is produced based on synthetic gum base, which is non-biodegradable and remains in the environment for a long time. Accordingly, chewing gum residue can be considered as a dangerous environmental pollutant. This research was set up to develop a bio-chewing gum based on “Saqqez (Bene resin)” as the source of biopolymers. The produced bio-chewing gum was evaluated for its biodegradability (over a 20-weeks course), condition in a simulated digestive system, and textural and sensory properties; the properties were also compared with those of synthetic chewing gum. Cutting capability and Texture Profile Analysis were both examined using a Texture Analyser TA.XT2i. The bio-chewing gum developed in this study was found to be viable as a good alternative to synthetic chewing gum due to the natural gum used in its production, as well as its good biodegradability and textural and overall acceptability. Read more
Researchers from the University of Queensland have been investigating texture-modified 3D printed dark chocolate in a sensory evaluation and consumer perception study. 3D printing of chocolate has yet to break through in the confectionery industry, partially due to substandard texture, so research and development in this area is very important. In this study, they used their TA.XTplus Texture Analyser to perform hardness tests on samples. The results obtained from the sensory tests and consumer survey provided a useful insight into consumers' perception of 3D food printing and the 3D product’s design. This awareness will be beneficial to promote this technology in the food industry. Find out more
Recent Research into the Texture Analysis of 3D Printed Objects in the Drug Industry
3D printing has taken off as a niche manufacturing method, enabling consumers to design and build their own goods. Although it has not lived up to the magnitude of some predictions of a decade ago, it holds an important place in the manufacturing industry. Objects can be built in any almost any format the consumer desires, and it has moved on from the early limitations of certain polymer groups as the building material. Now it is a potential tool in many industries, including bone and organ replacements, meat manufacture and even customisable bakery. As with any manufacturing innovation, the end product must go through a quality control process to assess its physical properties. A Texture Analyser is a crucial part of this procedure, giving a reliable way to test the mechanical properties of 3D printed objects. The following are a selection of recent publications into this interesting and important field.
Patient compliance in children can be low, particularly when a drug is bitter or intolerable. One particular study reports a simple, low cost and time-effective process for the development of a paediatric-friendly oral dosage form using 3D printed chocolate inks. They used their TA.XTplus Texture Analyser to perform Texture Profile Analysis of samples. The study reported on a facile method for the preparation of a 3D printed chewable chocolate-based dosage form with rapid and high release of both hydrophobic and hydrophilic drugs in simulated salivary fluid. The application of 3D printing technology was found to enable accuracy in dose adjustment, while at the same time introducing the potential of patient's active involvement in customisation of the design, textural and organoleptic properties of the final dosage form. Read more
Researchers from ETH Zürich have been investigating the development and characterisation of the processing steps of an ink for 3D printing for bone tissue engineering. Achieving reproducibility in the 3D printing of biomaterials requires a robust polymer synthesis method to reduce batch-to-batch variation as well as methods to assure a thorough characterization throughout the manufacturing process. Particularly biomaterial inks containing large solid fractions such as ceramic particles, often required for bone tissue engineering applications, are prone to inhomogeneity originating from inadequate mixing or particle aggregation which can lead to inconsistent printing results. In this study, the production of such an ink was optimised to assure homogeneous and reproducible printing results. They used their TA.XTplus Texture Analyser to perform extrusion force measurements. Extrusion force measurements were successfully used to predict the printability of inks. Read more
Researchers from Queen’s University Belfast have been investigating antioxidant PLA composites containing lignin for 3D printing applications as a potential material for healthcare applications. Interest in 3D printing for biomedical applications is increasing. This project focussed on developing low cost DIY fused filament fabrication printers and their use along with lignin-polylactic acid combinations. The breaking strength of filament samples was assessed using their TA.XTplus Texture Analyser in compression mode. This paper describes a simple method to combine the two polymers for 3D printing applications. A potential scenario for this material is as a wound dressing material due to the antioxidant activity of the composite material that can contribute to wound closure. Due to the low price of 3D printing equipment and its versatility, these materials can be used in hospitals to print wound dressings for patients on demand. Read more
Meanwhile other researchers from Queen’s University Belfast have been researching the development of a biodegradable subcutaneous implant for prolonged drug delivery using 3D printing. Implantable drug delivery devices offer many advantages over other routes of drug delivery. Most significantly, the delivery of lower doses of drugs, which potentially reduces side-effects and improves patient compliance. 3D printing is a flexible technique, which has been subject to increasing interest in the past few years, especially in the area of medical devices. The present work focussed on the use of 3D printing as a tool to manufacture implantable drug delivery devices to deliver a range of model compounds (methylene blue, ibuprofen sodium and ibuprofen acid) in two in vitro models. Five implant designs were produced, and the release rate varied, depending on the implant design and the drug properties. Additionally, a rate controlling membrane was produced, which further prolonged the release from the produced implants, signalling the potential use of these devices for chronic conditions. They used their TA.XT2 Texture Analyser to measure the mechanical properties of prepared implants using a three-point bend test. The results described in the present work demonstrate how 3D printing is a promising technology for drug eluting implant manufacture. Considering the simplicity of the technology described here, it can be easily transferred to a clinical setup, where implants could be designed on demand to fulfil patients’ needs after surgery. These implants may be suited for the delivery of drugs for localised treatment. For example, chemotherapy agents, antibiotics or local anaesthetics. Alternatively, they could be tailored by coating them for prolonged drug delivery for the treatment of chronic conditions. This can be done due to the versatility of 3D printing technology. Read more
Scientists from the University of Greenwich have been researching 3D printed microneedles for anticancer therapy of skin tumours. Over the last 20 years, microneedle devices have been used extensively for transdermal administration of various medicines in a non-invasive manner. Recent advances in the application of MN arrays to the skin involve the delivery of anticancer agents for the treatment of skin tumours. In this study, novel 3D printed polymeric microneedle arrays were fabricated for enhanced cisplatin delivery to A-431 epidermoid skin tumours for cancer treatment. They used their TA.HDplus Texture Analyser to measure the ability of MN arrays to penetrate skin. This study demonstrated the suitability of 3D printed microneedles in providing in-vivo transdermal delivery of anticancer drugs. Find out more
Researchers from the University of Nottingham have been investigating multi-material 3D bioprinting of porous constructs for cartilage regeneration. 3D printing can potentially benefit plastic and reconstructive surgeries by fabricating patient-specific tissue replacements with tissue-like functions and mechanical properties. One specific example in the field of plastic and reconstructive surgery is nasal reconstruction. This study aims to demonstrate the proof of concept of employing multi-material bio-printing to fabricate tissue replacements for nasal reconstructive surgeries. They used their TA.HDplus Texture Analyser to perform compression testing on samples to characterise their mechanical properties. The study showed the feasibility of manufacturing neocartilage using 3D bioprinted porous constructs which could be applied as a method for fabricating implants for nose reconstruction. Read more
Scientists from the Federal University of Piaui have been researching printed 3D hydrogel structures employing low-cost stereolithography technology. Stereolithography technology associated with the employment of photocrosslinkable, biocompatible, and bioactive hydrogels has been widely used. This method enables 3D microfabrication from images created by computer programs and allows researchers to design various complex models for tissue engineering applications. This study presents a simple and fast home-made stereolithography system developed to print layer-by-layer structures. They used their TA.XTplus Texture Analyser to perform unconfined compression tests on hydrogel samples. The 3D printed complex structures in this study highlighted the potential of this low-cost stereolithography technique as a great tool in tissue engineering studies, as an alternative to bioprint miniaturized models, simulate vital and pathological functions, and even for analysing the actions of drugs in the human body. Download the research paper
Scientists from the Technical University of Denmark have been researching 3D printed reservoir devices for oral drug delivery, from concept to functionality through design improvement for enhanced mucoadhesion. So far, microdevices for oral drug delivery have been fabricated as square or cylindrical reservoir structures with a localised and unidirectional release. The fabrication is usually carried out using sophisticated and costly microfabrication techniques. In this study, 3D printing of microreservoirs on sacrificial substrates is presented. This approach allows the devices to be accurately arranged in predetermined patterns, enabling implementation into batch production schemes in which the fabrication of the devices is linked to processing steps such as automated drug loading and sealing. Moreover, design and 3D printing of alternative geometries of minireservoirs featuring anchor-like surface structures for improved mucoadhesion and intestinal retention is demonstrated. They used their TA.XTplus Texture Analyser to perform mucoadhesion tests. Surface texturing of minireservoirs was found to increase mucoadhesion of the devices up to two-fold compared to a nonstructured control. The structuring also led to a strong bias in mucoadhesion in different orientations, which can facilitate a correct orientation of the devices and so lead to unidirectional release of drugs toward the intestinal mucosa for increased drug uptake. Find out more
Scientists from the University of Science and Technology Beijing have been researching a novel waterborne polyurethane with biodegradability and high flexibility for 3D printing. 3D printing provides a new approach of fabricating implantable products because it permits a flexible manner to extrude complex and customised shapes of tissue scaffolds. Compared with other printable biomaterials, polyurethane elastomers have several merits, including excellent mechanical properties and good biocompatibility. However, some intrinsic behaviour, especially a high melting point and slow rate of degradation, hamper their application in 3D printed tissue engineering. This study aimed to develop a 3D printable amino acid modified biodegradable waterborne polyurethane using a water-based green chemistry process. The flexibility of this material endows better compliance with tissue during implantation and prevents high modulus transplants from scratching surrounding tissues. They used their TA.HDplus Texture Analyser to perform mechanical tests on 3D printed samples. The study concluded that this printable polymer can be used as an alternative biomaterial for tissue engineering with low temperature printing, biodegradability and compatibility. Find out more
Texture Analysis in Research: Fish
According to Allied Market Research, the global seafood market is projected to reach $155,316 million by 2023, registering a CAGR of 3.6% from 2017 to 2023. Seafood is an excellent source of nutrition and provides numerous health benefits. A rise in awareness about these benefits is helping to drive the growth of the global seafood market, as well as other factors such as increasing disposable income, changing lifestyles and consumer diet preferences.
The majority of fish products sold on the market in the UK are prepared for direct cooking, which means that they are processed “pin-bone free”. Deboning is therefore an important step within the manufacturing process of fish. Scientists from Abertay University have been researching salmon and rainbow trout pin bones using Texture Analysis and micro x-ray computational tomography. This study assessed the length of pin bones from two fish species and two different industrial graded weights. They used their TA.XTplus Texture Analyser to measure the pulling force and break point of bone samples. This research has progressed the issues surrounding pin boning industrially. However, more studies are required in order to understand if these differences affect the overall deboning pin bone process. Read more
The fish market does not only include products destined for the dinner table. Fish proteins have interesting properties that can be exploited in other areas, including packaging applications.
The study of polymers from renewable and biodegradable sources is of great interest to replace petroleum-based plastics due to the concerns about environmental problems and the depletion of fossil resources. Myofibrillar proteins found in fish have a good film forming ability that leads to the formation of polymers for food packaging development. However, as with other bio-sourced macromolecules, they have limited performance compared to synthetic materials. Cold plasma represents a promising strategy to change their properties. Scientists from the Federal University of Rio Grande have been researching the effects of cold plasma were studied on the properties of fish protein films. They used their TA.XTplus Texture Analyser to measure the tensile strength and elongation at break of their samples, according to ASTM D882-02. Plasma application was found to affect the physiochemical properties, microstructure and thermal stability of samples, and time of plasma application was found to affect their mechanical performance. Read more
In a similarly environmentally-friendly application, researchers from Çukurova University have been investigating the physiochemical and functional properties of gelatine obtained from tuna, frog and chicken skins. Growing demand for gelatine has increased interest in using alternative raw materials. In this study, different animal skins were used in gelatine extraction, and quality characteristics and functional properties of the resultant gelatines were comparatively investigated. They used their TA.XTplus Texture Analyser to measure bloom strength of gel samples. Bloom value was significantly higher in frog skin gelatine compared to that of chicken and tuna skin gelatines. Results showed that processing waste like skins of different animals may present opportunities in gelatine production as high quality alternatives. This study may help the industry by providing comparable data over potentially significant sources. Find out more
Manufacturers often have motivation to remove fat from food products, but when something is removed from a recipe, it inevitably has to be replaced with another ingredient. Sometimes that replacement is another type of fat, or it might be another ingredient altogether (to reduce the overall fat content of the food). Food manufacturers have to test the altered food in comparison with its original form to ensure that all textural properties remain the same within acceptable limits.
Palm oil is an example of an ingredient that is frequently being replaced in food this decade. It is the oil extracted from the fleshy interior layer of the fruit of oil palms. According to “Trends in Global Palm Oil Sustainability Research.” in the Journal of Cleaner Production, it is the most produced vegetable oil in the world. In food manufacture, it is used as a flavour and moisture additive, an emulsifier and a lubricant. However, concerns over child labour, deforestation (and the associated decline in animal populations) and climate change have driven many manufacturers to reduce its inclusion in their products, as well as looking to reduce the high saturated fat content it gives to food. This is also an area of interest in scientific research, with efforts focussed on the change in physical properties and taste before and after palm oil’s replacement. Texture Analysis is central to the research and development of products subject to palm oil removal. Some supermarkets and manufacturers have recently had campaigns to entirely remove palm oil from their own brand products to meet with the growing public distaste for the ingredient, whether from an environmental or health perspective.
The replacement of trans fats and saturated fats due to health concerns has long been an area of interest in the food industry, and environmental concerns can be a further push for oils of tropical origin. Scientists from the University of Guelph have been researching methylcellulose structured oils as an alternative to palm oil shortening in sandwich cookie creams, putting their TA.XT2 Texture Analyser to use in Texture Profile Analysis of cream samples. It was found that varying the proportion of replacement oils had a large effect on the hardness, stickiness and gumminess of creams. Read more
Meanwhile, in Thailand, researchers from King Mongkut’s Institute of Technology Ladkrabang have been testing palm oil free cookies. The main objective of this study was to develop coconut oil based cookies fortified with tuna bone bio-calcium as a healthy food, rich in medium chain fatty acids and dietary calcium. After the ingredient swap, the quality and sensory properties of the samples were determined, including colour, diameter, thickness and hardness (which was tested using their TA.XTplus Texture Analyser). All tested properties of the cookies varied with levels of bio-calcium powder and coconut oil. It was found that 12% bio-calcium powder could be fortified into cookies using coconut oil as shortening replacer without any adverse effects on sensory properties. Read more
Over in Brazil, the focus is on reducing palm fats in hamburgers. A diet with high fat intake can lead to health problems, but fat is important to the texture of many foods. Scientists from the Federal University of Lavras have been researching hamburgers with chia seed added to act as a fat replacement. In this study, chia seeds were added in different quantities to chicken burgers to replace pork fat, and the resulting product investigated in terms of sensory characteristics. They used their TA.XTplus Texture Analyser to perform shear force measurements on samples. Although sensory taste scores and overall acceptance were reduced on products with higher chia addition, the degree of acceptance of the products was high. Results of this study highlighted the potential use of chia seed in the development of low fat and enriched dietary fibre burgers. Read more
According to Statista, the global dental market is projected to grow to around 37 billion dollars by 2021, and current indicators show that the market will keep moving forward, primarily driven by the implant sector. Its success is due to progress in the fields of medical technologies and implant materials.
When ceramic structures are used in the mouth, there is often a risk of wear between teeth and the ceramic part. Scientists from Boston’s University School of Dental Medicine have been researching this effect when different dental ceramic systems are used. Disc shaped specimens were held in resin and they used their TA.XTplus Texture Analyser along with a multiple sample vertical friction wear device to perform wear simulation. No differences were found in the linear and volumetric reduction of enamel cusps abraded against enamel disks or ceramic specimens. Read more
Meanwhile, Mars Inc. have been fabricating animal jaws. They have recently released a patent, entitled ‘Animal dentistry apparatus and methods’. Chewable products are often used to improve the oral hygiene of animals as the chewing action can help to remove plaque. It is useful to understand the mechanical properties of these products as they can affect their performance in cleaning teeth; existing mechanical measurement techniques involve their compression with cylindrical probes. This patent addresses the shortcomings of in-vivo measurements with existing test methods for chewable products. They used their TA.HDplus Texture Analyser to perform tests with a mechanical jaw assembly. Read more
Over in Hangzhou, researchers from Zhejiang Gongshang University have been investigating the locking up of food between posterior teeth and its influence on chewing efficiency. Food particles are intra-orally locked up between antagonistic posterior teeth during each chewing cycle, and this can affect the selection of particles for subsequent breakage, hence also affecting chewing efficiency. The two aims of this study were to determine the extent of locking up and to examine the relationship between locking up and chewing efficiency. The researchers used their TA.XTplus Texture Analyser to perform penetration tests on sheet bolus samples. Relationships between locking up and chewing efficiency were successfully found. Read more
Scientists from Zhejiang University of Technology have been researching the fabrication and evaluation of dental fillers using customised moulds via 3D printing technology. In view of the high incidence and long-term treatment of dental caries, personalized dental fillers with long therapeutic action have broad application prospects in the dental clinic. The objective of this study was to fabricate and evaluate novel dental fillers using state-of-the-art 3D printing technology. To mimic the support from peripheral tooth tissue, the compression behavior of the optimal dental filler was determined with customized compression molds designed according to the printed mold, using their TA.XTplus Texture Analyser. The study confirmed that 3D printing was successful in designing and fabricating personalised dental fillers with high mechanical strength and “on-demand” drug release characteristics. Read more
To read more about dentistry applications using a Texture Analyser click here.
Texture Analysis in Research: Meat
Collagen is the major fibrillar component and protein in both human and animal connective tissue. It is applied in medical preparations such as wound dressings and tissue engineering.
Meat and poultry production industries result in large amounts of organic waste, rich in collagen. Scientists from the University of Oslo have been investigating collagen from turkey tendons as a promising sustainable biomaterial for pharmaceutical use. The aim of this study was to isolate and characterise pepsin soluble collagen from turkey tendons.
Mechanical properties of samples were studied using their TA.XT2i Texture Analyser in compression mode. This study illustrated a potential sustainable use of leftover raw materials from poultry. Read more
The popular hamburger continues to thrive in many new and reformulated guises. It is well know that whilst fat is important to the texture, usually a diet with a high fat intake from the consumption of such products can lead to health problems.
With this in mind, scientists from the Federal University of Lavras have been researching the technological and sensory characteristics of hamburgers with chia seed added to act as a fat replacement. In this study, chia seeds were added in different quantities to chicken burgers to replace pork fat, and the resulting product investigated in terms of sensory characteristics, among others.
They used their TA.XTplus Texture Analyser to perform shear force measurements on samples. Lower sensory taste scores and overall acceptance were conferred on products with higher chia addition, although the degree of acceptance of the products was high. Results of this study highlighted the potential use of chia seed in the elaboration of low fat and enriched dietary fibre burgers. Read more
Meanwhile, scientists from Tallinn University of Technology have been researching the influence of different packaging materials and atmospheric conditions on the properties of pork rinds. Pork rinds are a popular and nutritious snack food in many countries.
This study investigated the rancidity and texture of samples during a 120-day shelf life period under different atmospheres and packaging conditions. They used their TA.XT2i Texture Analyser to investigate the hardness and crispness of samples with a 3mm penetration probe. The study was successful in determining the optimum packaging and atmosphere for preserving pork rind samples. Read more
To review the typical types of tests used in the meat industry for texture measurement visit our Meat and Fish Testing page.
Alternatively request our article that gives an overview of all of these methods for meat testing.
The study of the mechanical properties of soft tissues is valuable to evaluate the progress of diseases such as tumours and treatment effects, to simulate medical surgeries, to understand the aging process and to evaluate the efficacy of cosmetic products. Yet again, the Texture Analyser has proven to be an invaluable tool in the measurement of such samples.
Recently researchers from the National University of Colombia have investigated the influence of indentation test factors on the mechanical response of skin. This study proposes in vivo tests and design of experiments to determine the influence of experimental factors on the mechanical response of soft tissue. They used their TA.XT2i Texture Analyser to perform indentation measurements on forearm skin. Read more
The same researchers have also published an article regarding the incidence of temperature and indenter diameter on the mechanical response of skin during indentation tests. Read more
Real- time surgical simulation is of growing scientific interest. Researchers from the University of East Anglia have been investigating a hyperelastic finite element model of human skin. Their work presents a ‘full cycle’ study on the interactive simulation of plastic surgery interventions. The study was initiated by performing in-vitro experiments on human skin, the data of which were fit to various computer models. They used their TA.XT2 Texture Analyser to perform tensile tests on skin samples. The study was successful in modelling deformation of human skin. Read more
Meanwhile in the field of drug delivery through skin, researchers from Queen’s University Belfast have been investigating optical coherence tomography as a valuable tool in the study of the effects of microneedle geometry on skin penetration characteristics and in-skin dissolution. Microneedle arrays are used to pass drugs through the skin in a minimally invasive way. This study looked into the effect that needle geometry and force of application have on penetration characteristics of soluble polymer arrays into porcine skin. They used their TA.XTplus Texture Analyser to apply load to a spring-loaded piston for application of the microneedle arrays. The successful use of optical coherence tomography in this study could prove to be a key development for polymeric microneedle research, accelerating their commercial exploitation. Read more
In the same field, researchers from Loughborough University have been investigating the influence of array interspacing on the force required for successful microneedle skin penetration, using theoretical and practical approaches. The insertion behaviour of microneedle arrays depends on the mechanical properties of the skin and the microneedle geometry and distribution. In addressing this issue, this paper studies the mechanism of microneedle array insertion into the skin and provides a simple quantitative basis to relate the insertion force with distance between two microneedles. They used their TA.XTplus Texture Analyser to measure the force of insertion of arrays at two different speeds. Results from theoretical analysis and finite element modelling agreed well with experimental results. This showed that microneedle interspacing only began to affect insertion force at low interspacing. This model provides a framework for optimising microneedle devices, and should aid the development of suitable application methods and determination of force for reliable insertion into skin. Read more
To characterise the tactile properties of residual film of topical products applied to skin, scientists from Normandy University have been researching instrumental and sensory methodologies. Cosmetic and pharmaceutical topical products were selected based on their various texture, galenic form and composition. Key texture attributes such as firmness, stickiness, spreadability and the amount of residue were objectively evaluated using sensory analysis. Additionally, texture analysis (compression tests using a TA.XTplus Texture Analyser), rheology and tribology were carried out. The investigation was successful in showing how the tactile properties of topical gels and emulsions are studied using complementary tests in order to understand and improve the skinfeel of topical preparations. Read more
Those readers engaged in research in these activities may be interested in an article entitled ‘Using texture analysis to quantify the efficacy of skin care products’ by Stable Micro Systems. Addressing such issues as skin tightening and the use of the texture analyser for indentometric testing, this feature is available free of charge on request.
To request your PDF copy, visit our Resource Request page
With 9.6 billion people forecast to inhabit the planet in 2050, scientists have warned that population growth could lead to an unsustainable increase in food production if consumption patterns persist. Considering the rising world population and the scarce water and land resources, it is extremely important to find new and sustainable ways to produce food. Edible insects are particularly interesting due to their high protein content and lower environmental impacts compared to traditional livestock. They have been promoted as a source of nutrients able to contribute to the increasing need of animal protein in an environmentally sustainable fashion. In general, insects contain a considerable amount of protein with a well-balanced amino acid spectrum, a high amount of lipid, and a noteworthy content of micronutrients such as copper, zinc, and iron.
Researchers from Wageningen University & Research have been performing an investigation toward the design of an insect-based meat analogue, specifically the role of calcium and temperature in the coagulation behaviour of Alphitobius diaperinus proteins. This study focused on the coagulation behaviour of protein from larvae of Alphitobius diaperinus. The effect of incremental CaCl2 concentration and temperature on physical-chemical properties of insect coagula was investigated. The textural properties of the coagulum were measured in compression using a TA.XTplus Texture Analyser. The results of this study provide important information for the product development of insect protein-based meat analogues. Read more
In the bakery industry, muffins are one of the most popular high-calorie snack products consumed worldwide. As a response to growing consumer interest in healthy nutrition, the food industry is increasingly focused on designing foods with reduced sugar content. Insects can be used as a matrix for the introduction of various nutrients, such as protein and antioxidants. The use of protein enrichment, on the one hand, reduces the sugar content of the product, but, on the other hand, it may also have a significant impact on its textural properties.
Cricket powder may be used as a protein-rich additive. Researchers from Poznań University of Life Sciences have been investigating the effects of the replacement of wheat flour with cricket powder on the characteristics of muffins. They used their TA.XTplus Texture Analyser to perform texture profile analysis on the muffin samples. Slight changes to colour and textural properties were found after the addition of cricket powder. However, it was found to be suitable for use in the enrichment of muffins with protein without reducing the sensory attractiveness of the product obtained. Find out more
Meanwhile, researchers from the Federal University of Rio Grande do Sul have been investigating cricket powder (Gryllus assimilis) as a new alternative protein source for gluten-free breads. This study evaluated the use of cricket powder as protein source for the production of gluten-free bread in comparison with two other protein sources: buckwheat and lentil flours. They used their TA.XTplus Texture Analyser to perform Texture Profile Analysis on bread slices. Results confirmed that the enrichment with cricket powder can lead to the production of gluten-free bread with acceptable technological properties and high protein content. Find out more
Scientists from the National Agriculture and Food Research Organisation, Japan, have been researching compression tests of soft food gels using a soft machine with an artificial tongue. Easy to eat food is increasingly required in the advanced-aged society in Japan. Mechanical properties of such foods must be modified such that the foods are easily broken by the tongue without chewing. When foods are compressed between the tongue and the hard palate, the tongue deforms considerably, and only soft foods are broken. To simulate tongue compression of soft foods, artificial tongues with stiffness similar to that of the human tongue were created using clear soft materials. The scientists in this study used their TA.XTplus Texture Analyser to perform compression tests on cylindrical samples. The fracture properties measured using the soft machine were better than those obtained from a conventional test between hard plates to mimic natural oral processing in humans. The fracture force on foods measured using this soft machine may prove useful for the evaluation of food texture that can be mashed using the tongue. Read more
Scientists from the Department of Food Science, University of Tennessee, have been investigating the characterisation of oral tactile sensitivity and masticatory performance across adulthood. In a society that is rapidly aging, it is important to understand the subtle changes in physiology and eating behaviour that are associated with aging. This study used a variety of tests of oral sensitivity to better understand which aspects of oral physiology are integral for effective chewing.
Two main measures of oral sensitivity were performed: to assess bite force, subjects were asked to discriminate between foam samples of varying hardness. Second, to assess lingual sensitivity the subjects were asked to identify 3D printed shapes using their tongue, as well as identify confectionery letters. Additionally, masticatory performance was measured through assessing each participant’s ability to mix two‐coloured chewing gum. The researchers used their TA.XTplus Texture Analyser to verify sample hardness levels.
Sensitivity and masticatory performance in the younger age groups was superior to that of older adults but results suggested that age‐related declines in bite force sensitivity were not a significant cause of altered masticatory performance. This study represents a valuable first step in showing that bite force sensitivity does not depend on age, and the minimal influence of factors such as oral sensitivity on masticatory performance. Read more
By 2025, the world will have almost 800 million people over the age of 65.
The UN estimates that the global population age 60+ will soar from 11% in 2000 to 22% by 2050.
While age is just a number, the numbers are certainly on the rise. Yet another challenge is that sensory perceptions necessary for the palatability of food – sight, touch, smell, and taste – diminish as humans age.
Taste is the most important factor for all consumers, but texture of food products may be a greater concern for older consumers than younger ones because of difficulty in chewing and swallowing.
How can texture analysis help? Request our article on Designing foods with specific health claims for an ageing population
Designing the best potato chip
Researchers have developed a method to analyse the physical characteristics of a potato chip at four stages of eating — from the first bite to the final swallow — to help formulate a tastier low-fat snack. The results of the research have been reported in the Journal of Agricultural and Food Chemistry.
While munching on low-fat potato chips might reduce the guilt compared with full-fat versions, many people don’t find the texture as appealing. Cutting fat in potato chips usually involves reducing the vegetable oil content but it’s the oil that helps give the product its characteristic crunch, taste and mouthfeel.
Texture perception is conceptualised as an emergent cognitive response to food characteristics that comprise several physical and chemical properties. When food scientists formulate a new low-fat chip, they often rely on trained sensory panellists to tell them how well the new snack simulates the full-fat version. This process can be expensive, time-consuming and often subjective, since perceptions can vary based on factors like a person’s saliva flow rate and composition
Read more about what mechanical testing was performed in this research and how the new technique to link physical measurements with sensory perceptions could be used.
Meanwhile, scientists from the Korea Food Research Institute have been researching the prediction of sensory crispness of potato chips using a reference-calibration method. Reference calibration is a useful technique when sensory evaluation is not feasible or practical. This study was conducted to predict the crispness perception of potato chips evaluated by instrumental means through the reference-calibrated method. They used their TA.XTplus Texture Analyser to perform compression and three-point bend tests. The relationship between the instrumental graph area and the sensory crispness of the standard references was found to be nonlinear over the standard crispness scale but the Fechner model was suitable for predicting the sensory crispness of chips. This study suggests that standard references with a reference-calibration method can be used to calibrate the crispness of potato chips.
Scientists from the Thomas More University of Applied Sciences have been researching the use of a Texture Analyser to objectively quantify foot orthoses.
Foot orthoses alter the kinematics and kinetics of gait. With increasing importance of evidence-based practice and with the permanent development of subtractive manufacturing and introduction of additive manufacturing, there is a growing need for the quantification of orthoses parameters. This paper describes a measurement method and protocol to quantify different parameters of a foot orthosis. They used their TA.XTplus Texture Analyser to perform indentation tests on orthoses. Results showed the added value of the proposed technique as the parameters were not only defined by the material, but also by the shape.
Meanwhile, scientists from Arizona State University have been researching light-activated tissue-integrating sutures (LATIS) as surgical nanodevices.
Sutures are typically the primary means of soft tissue repair in surgery and trauma. Despite their widespread use, sutures do not result in immediate sealing of approximated tissues, which can result in bacterial infection and leakage. Non-absorbable sutures and staples can be traumatic to tissue, and the trauma can be exacerbated by their subsequent removal. Use of cyanoacrylate glues is limited because of their brittleness and toxicity.
In this work, laser‐activated tissue‐integrating sutures are described as novel nanodevices for soft tissue approximation and repair. They used their TA.XTplus Texture Analyser to perform tensile tests on fibre samples. The results of this study indicated that LATIS‐facilitated approximation of skin in live mice synergises the benefits of conventional suturing and laser‐activated tissue integration, resulting in new approaches for faster sealing, tissue repair, and healing.
Scientists from the University of Michigan have been investigating the mechanics of scaling-up multichannel scaffold technology for clinical nerve repair.
Peripheral nerve injury remains a large clinical problem, with challenges to the successful translation of nerve repair devices. One promising technology is the multichannel scaffold, a conduit incorporating arrays of linear microchannels, which has high open lumen volume to guide regenerating nerves towards distal targets.
To maximise open lumen volume, and scale-up scaffolds for translation, this study explored how mechanical properties were affected by material choice, microstructure and channel architecture. They used their Texture Analyser TA.XTplus to perform tests in compression and tension. The study demonstrated significant progress towards translation and will bring multichannel technology closer to the clinic.
3D printed food
Personalisation has been pointed as the driving force to disrupt traditional ways to produce and deliver food.
Three-dimensional food printing (3DFP) is constantly associated as a potential alternative to achieve personalisation and enchant a variety of customers.
By means of extrusion-based 3DFP, for example, three main features can be acquired that cannot be done using conventional casting methods of paste-like materials: (1) the design of internal structures (infill percentages and internal variations of the nutritional content); (2) encapsulation of probiotics, vitamins and nutrients; and (3) freshly mixing of ingredients to ensure the ideal texture within a complex 3D construct (in dual or multiple nozzle systems). An Introduction to the Principles of 3D Food Printing is a book that has just been published which uses a Texture Analyser to measure the properties of such solid food constructs. This chapter focusses on reporting the different types of 3D printing techniques and assessment of printing quality. Insights were given on the choice of the 3DP technique, based on the material properties, applicability and postprocessing requirements.
Researchers from the University of Queensland have been investigating the textural modification of 3D printed dark chocolate by varying internal infill structure. They used their TA.XTplus Texture Analyser to perform textural characterisation of the samples with a knife blade. A higher force was required to break samples with a higher infill percentage. This technique was found to be a powerful tool in controlling the mechanical properties of 3D printed food in general.
Meanwhilte, researchers from the Chinese Academy of Agricultural Sciences have been investigating the application of soy protein isolate and hydrocolloid based mixtures as promising food materials in 3D food printing. Rheological properties, printability and 3D printed geometries of soy protein isolate mixtures with sodium alginate and gelatin were investigated. The SPI and their mixtures showed shear thinning behaviour and can be used as an ideal material for 3D printing. The mechanical properties of printed protein mixture cylinders were investigated using their TA.XT2i Texture Analyser. The addition of sodium alginate and gelatin to SPI were found to cause no chemical cross-linking between protein subunits during mixing and 3D printing at 35°C, while improving the hardness and chewiness of 3D printed geometries. The overall results suggested that the food matrix of SPI, sodium alginate and gelatin will be a promising material in 3D food printing.
Food materials for FDM printing should have adequate rheological properties that can be easily extruded and maintain their shape. However, there are very few foods that meet this condition and it is still a challenge to process many food materials to be applicable to this method. Vegetables are a typical non-printable traditional food material due to their excessive moisture and low carbohydrate content, and lack of proteins that give proper rheological properties. Scientists from the College of Life Science and Biotechnology, Korea University, have been researching the effect of particle size on the 3D printing performance of the food-ink system with cellular food materials. Recently, there has been increased interest in the 3D printing of food due to the availability of design freedom of texture, shape, composition, taste and flavour. Fused deposition modelling (an extrusion-based technology) is the most commonly-used technique for food fabrication. They used their TA.XTplus Texture Analyser to perform Texture Profile Analysis and standard compression tests. The results obtained in this study suggest that increasing the particle size of the incorporated food powder can achieve efficient mechanical strength increase. This may be useful in determining parameters which are required to prepare the food-ink system such as the milling time and the maximum incorporation content of the food powder.
For application in the meat industry, scientists from the University of Queensland have been researching the post-processing feasibility of composite-layer 3D printed beef. Post-processing feasibility studies the integrity of the designed internal and external structures of 3D printed products. This study examined the effect of infill density and fat content on the post-processing physical changes and texture of lean meat-lard composite layer 3D printed meat products cooked sous-vide. They used their TA.XTplus Texture Analyser to perform puncture tests and Texture Profile Analysis. Overall, increasing the fat content (or lard layers) resulted in higher cooking loss, shrinkage, and cohesiveness, and lower fat retention, moisture retention, hardness, and chewiness. On the other hand, an increase in infill density led to higher moisture retention with lower shrinkage and cohesiveness, resulting in higher hardness and chewiness.
Apricots have a short storage life principally caused by a rapid softening, which increases the sensitivity of the fruit to mechanical damage, and to the development of fungal diseases.
The current methods to assess fruit firmness give limited information on the evolution and the mechanisms of softening. Scientists from the Agroscope Research Centre have been researching a multi-parameter approach for apricot texture analysis. With the aim of developing novel strategies to better monitor fruit softening, a multi-parameter approach measuring textural properties was evaluated and compared to a reference method whose results are obtained from a unique parameter.
Quantitative measurement of texture is essential to ensure an optimal commercial quality of apricots on the market and to characterise the mechanisms involved in the evolution of this parameter before and after harvest. Thanks to a better understanding of the textural properties of apricots and their changes as the fruit ripens, quality for the consumers could be improved and losses reduced along the entire supply chain.
They used their TA.XTplus Texture Analyser to determine whole fruit firmness using a compression test. Measurements performed with the TA.XTplus Texture Analyser allowed a multi-tests approach that described more precisely the influence of cultivar and storage conditions on different textural properties of the fruit. This instrument gives whole curves from which parameters can be computed. This has the advantage that the evaluation of the influence of the different factors can be done based on the whole curves or only on the extracted parameters. Unlike measurements performed on an AGROSTA®100 device on a small surface of each fruit, compression tests are done on the whole fruit. This test gives information on the viscoelastic properties of the apricot, which is particularly useful for predicting its ability to resist to pressure forces occurring during the post-harvest handling of the fruit (during transport for example). Also, the results obtained by puncture tests allowed more precise evaluation of the influence of the storage conditions on the textural properties of the skin and the flesh. Moreover, texturometry allowed more detailed analysis of the properties of the skin which were not correlated with the firmness obtained with the manual device.
The results showed that this multi-parametric approach allows detailed evaluation of the apricots’ textural properties – after all why settle for an instrument that measures one parameters when you can benefit from a single universal instrument that has a multitude of texture measurement solutions?
Read our article ‘A world of food development possibilities with fruit’which presents a wide range of different texture measurements using the Texture Analyser on fruit ranging from dried, pureed, whole or processed. Request this article
3D printing applications
At the University of Milan scientists have been researching 3D printed multi-compartment capsular devices for two-pulse oral drug delivery.
The resistance to deformation of printed and moulded capsular devices was measured under compression using their TA.XTplus Texture Analyser.
This study helped to develop delivery methods for enhanced customisation of drug combinations.
Orodispersible films (ODFs) are promising dosage forms for children or elderly people. By printing active pharmaceutical ingredients onto orodispersible films, the flexibility of drug dosing is increased and provides potential for personalised medicines. Scientists from Heinrich Heine University Dusseldorf have been researching printing methods for pharmaceuticals by inkjet technology. This study deals with the technology transfer from a small-scale inkjet printing system to a pilotscale process. They used their Texture Analyser TA.XTplusto measure the elongation to break and puncture stress of the samples, both of which were affected by the number of layers and the amount of ink used. The results showed that multiple printing has a huge impact on the mechanical properties of the film, leading to the conclusion that the ink formulation and the number of printed layers should be carefully selected. The continuous ODF production with direct printing enabled various printing concepts, which may serve for individualised dosing in personalised medicine treatment in the near future.
Meanwhile scientists from Åbo Akademi University have been researching additive manufacturing of personalised orodispersible warfarin films. Warfarin is a narrow therapeutic index drug that requires personalised dosing which is currently not achieved by marketed products. Further, paediatric and geriatric patients may face swallowing problems with solid oral dosage forms. To face these issues, the aim of the present study was to investigate semisolid extrusion 3D printing for production of warfarin containing orodispersible films. They used their TA.XTplus Texture Analyser to determine the burst strength and flexibility of the films. Extrusion 3D printing was successfully utilised to produce transparent, smooth and thin, yet flexible and strong orodispersible films containing therapeutic doses of warfarin. Excellent linearity between the designed sizes of the films and the drug contents was achieved indicating semisolid extrusion 3D printing as a promising way to produce orodispersible warfarin films with personalised doses.
In Switzerland, researchers from ETH Zurich have been investigating 3D printing of a wearable personalised oral delivery device. Despite the burgeoning interest in three-dimensional (3D) printing for the manufacture of customisable oral dosage formulations, a U.S. Food and Drug Administration–approved tablet notwithstanding, the full potential of 3D printing in pharmaceutical sciences has not been realised. In particular, 3D-printed drug-eluting devices offer the possibility for personalisation in terms of shape, size, and architecture, but their clinical applications have remained relatively unexplored. These researchers used 3D printing to manufacture a tailored oral drug delivery device with customisable design and tunable release rates in the form of a mouthguard and, subsequently, evaluated the performance of this system in the native setting in a first-in-human study. They used their TA.XTplus to determine the tensile strength of the filaments. The elastic modulus was calculated from the slope of the stress-versus-strain curve in the linear region. This proof-of-concept work demonstrates the immense potential of 3D printing as a platform for the development and translation of next-generation drug delivery devices for personalised therapy.
Due to consumers now hating plastic, waste companies are being forced to find alternative solutions.
The holy grail of packaging development is now to present a recyclable, compostable, biodegradable and environmentally friendly solution which does not compromise on packaging integrity and desired performance.
Researchers from the National University of Trujillo have been investigating biodegradable foam trays based on starches isolated from different Peruvian species. In this study, sweet potato, oca, and arracacha starches were used to produce foam trays by a thermopressing process as a sustainable alternative to expanded polystyrene. They used their TA.HDplus Texture Analyser to determine the tensile strength and elongation of the trays according to ASTM D828-97. Arracha starch was found to produce trays with low density, good mechanical resistance and thermal stability, whereas sweet potato and oca starch produced foam trays with the highest mechanical resistance.
Food consumption trends and packaging technologies are developing quickly, with environmental concerns driving product advancements and shift in consumer demand trends. Researchers from the National University of La Plata have been investigating edible flavoured oven bags for cooking meat based on proteins. There are several brands in the market that sell oven bags for cooking based on different synthetic polymers. Those intended for cooking meat would have the advantage of maintaining the authentic flavour of the food, since they would retain their natural aromas, minerals and vitamins. They also avoid the use of cooking oil and keep the oven clean once the bag is removed together with the food. This work deals with the activation of protein films with a flavouring and their evaluation as oven bags for cooking meat. They used their TA.XT2i Texture Analyser to measure heat seal strength according to ASTM F88-00. The same instrument was used to measure the texture of cooked chicken meat. Bags made with soybean protein isolates successfully resisted cooking, but those made with bovine gelatin disintegrated during cooking. Furthermore, soybean protein bags transferred the flavour to chicken meat during cooking, without affecting their texture and water content.
Here are several examples of the use of Texture Analysis in cosmetic product development...
Researchers from Chanel Beauty Perfumes, Beauty and Innovation Research, have been investigating the relations between the sensory properties and fat ingredients of lipsticks.
Lipstick is a flagship make-up product with over 900 million units sold per year worldwide, including 300 million in Europe. It is the best-selling cosmetic product.
Although a consumer will buy a lipstick according to the colour and the make-up effect, she will only buy the same one again if she is attracted by the sensory nature of the product. Sensory properties such as slipperiness, smoothness, thickness of the coating, and a moisturising sensation are strategic criteria in repeating the purchase.
The lipstick bending force was measured using a TA.XTplus Texture Analyser coupled with a Lipstick Cantilever Rig. The results of this study confirm the major role of the viscosity of oils and the wax used in the formula on the sensory and mechanical properties of the lipstick. It is therefore possible to modify the sensory properties, for example to adjust the shininess of a lipstick, without altering its mechanical resistance. This opens up opportunities for developing innovative sensory textures in short lead times.
Meawhile, scientists from Normandy University have been researching the prediction of residual film perception of cosmetic products using an instrumental method and non-biological surfaces, with the example of stickiness after skin application..
The cosmetics market is very competitive, with a huge number of attractive products. To be distinguished from competitors, a cosmetic product has to be efficient but also pleasant to use, through its colour, fragrance and texture. The aim of this work is to investigate how residual sensory properties of cosmetic products can be predicted without using a panel of assessors, focusing on the residual film attribute “stickiness”.
They used their TA.XTplus Texture Analyser to evaluate the adhesive property of residual film samples. Results strongly suggested that the physical stimulus responsible for cosmetic film stickiness can be instrumentally measured on both in vivo skin and artificial skin.
In the bakery industry, formulations continue to be tested that replace an ingredient (such as gluten) or supplement (e.g. soybean or soy protein) to enhance a product.
The following are recent publications highlighting the use of a texture analyser to measure the effects of such formulation change.
Scientists from Nanjing University of Finance and Economics have been researching the effects of whey and soy protein addition on the rheological properties of wheat dough.
Since it is known that the gluten network is responsible for viscoelastic properties in wheat dough and for dough structure strength and gas retention, most studies reported that enrichment of foreign proteins interfered with gluten development and so had negative effects on bread quality. This study compared the effects of whey and soy proteins on the thermomechanical, dynamic rheological and microstructural properties of wheat dough and bread-making quality in a relatively wide range of protein addition (0–30%).
They used their TA.XT2i Texture Analyser to perform texture profile analysis on breadcrumbs. The results suggested that selection of the protein source and amount with appropriate functionalities significantly affected the structure of the dough and quality of the bread.
This study is essential for product development and process control when considering the popularity of protein fortified bakery products.
Researchers from Monterrey Institute of Technology have been investigating rheology, acceptability and texture of wheat flour tortillas supplemented with soybean residue.
Dry soybean residue is a by-product rich in dietary fibre and protein with high levels of essential amino acids. This study investigated the effects of the substitution of refined wheat flour with dry soybean residue in dough rheology and hot-press tortilla texture, dimensions, colour, protein and dietary fibre contents.
They used their TA.XT2i Texture Analyser to perform texture profile analysis on optimally developed doughs. Results indicated that wheat flour tortillas with 10% soybean residue were an excellent alternative to regular counterparts owing to their higher dietary fibre and protein quantity and quality.
Scientists from the University of Bologna have been researching the influence of the addition of soy product and wheat fibre on rheological, textural, and other quality characteristics of pizza.
In this work, the effects of using new ingredients (e.g., soy paste, wheat fibre) on the rheological, textural, physicochemical, nutritional, and organoleptic characteristics of an enriched pizza type were investigated both at laboratory and industrial levels using their TA.HDi Texture Analyser to perform physical testing on dough samples. The new pizza provides a product that combines solid technological performances, in terms of rheological properties and dough elasticity, with improved and balanced nutritional quality, thanks also to the ingredients used in the topping.
Results demonstrate the possibility of obtaining new pizza products characterised by nutritional and sensorial properties tailored for different groups of consumers.
A patent has also recently been released by Campbell Soup Company, entitled ‘Gluten Free Compositions and Methods for Producing Shelf-Stable Breads and Other Bakery Products’.
New bread flour substitute compositions were outlined including starch and hydrocolloid blends. The freshness (staling) of bread is generally monitored by measuring the changes in firmness of loaf over its shelf life, and their TA.XTplus Texture Analyser was used to perform these measurements according to the AACC method. Amylose reduced gluten free breads were found to have consistently lower firmness values than the control gluten free bread.
Testing coronary stents
Scientists from Nantes University Hospital have been researching standardised bench test evaluation of coronary stents and their biomechanical characteristics.
The purpose of the study was to develop a standardised and global bench test protocol to evaluate the biomechanical characteristics of the most currently used drug‐eluting coronary stents. The use of coronary stents has contributed to the reduction of cardiovascular mortality but can be associated with specific complications. Improving the biomechanical matching between the stents and the coronary anatomy may reduce these complications.
Flexibility (crimped and deployed stents) and longitudinal and radial resistances were evaluated using a TA.HDplus Texture Analyser. Biomechanical characteristics were significantly different for all tested devices. This should be taken into consideration to select the most appropriate device for each clinical situation.
Scientists from the Swiss Federal Institute of Technology in Zürich have been performing a comparative study of cartilage engineered constructs in immunocompromised, humanised and immunocompetent mice.
Choosing the best ectopic in vivo model for cartilage engineering studies remains challenging and there is no clear consensus on how different models compare to one another. The use of xenogenic cells can often limit the choice to immunocompromised animals only and so prevents the understanding of how tissue-engineered grafts perform with potential active inflammatory and immunological responses.
The aim of this study was to evaluate the chondrogenic potential of a recently developed hydrogel in four mouse strains with varying immune systems. Scaffolds were tested under unconfined compression using their TA.XTplus Texture Analyser. The results of this study showed that it is possible to engineer a cartilage-like graft subcutaneously not only in immunocompromised, but also in immunocompetent and humanised mouse models.
Testing films for wound healing applications
Researchers from the Federal University of Pelotas have been investigating a polysaccharide-based film loaded with vitamin C and propolis as a promising device to accelerate diabetic wound healing.
Wound healing can be a painful and time-consuming process in patients with diabetes mellitus. In light of this, the use of wound healing devices could help to accelerate this process. In this research, cellulose-based films loaded with vitamin C and/or propolis, two natural compounds with attractive properties, were engineered.
Mechanical properties were investigated by tensile testing using a TA.XT2 Texture Analyser. The results of this study showed that these novel eco-friendly films may represent a new therapeutic approach to accelerate diabetic wound healing.
At the grocery store, most foods — meats, breads, cheeses, snacks — come wrapped in plastic packaging.
Not only does this create a lot of non-recyclable, non-biodegradable waste, but thin plastic films are not great at preventing spoilage – and some plastics are suspected of leaching potentially harmful compounds into food. Current food packaging is mainly petroleum-based, which is not sustainable. It also does not degrade, creating tons of plastic waste that sits in landfills for years – an issue that is now weighing heavily on the minds of all consumer after recent documentaries.
To address these issues, scientists are now developing a packaging film made of milk proteins — and it is even edible. To create an all-round better packaging solution, Dr Peggy Tomasula and colleagues at the U.S. Department of Agriculture are developing an environmentally friendly film made of the milk protein casein. These casein-based films are up to 500 times better than plastics at keeping oxygen away from food and, because they are derived from milk, are biodegradable, sustainable and edible.
Some commercially available edible packaging varieties are already on the market, but these are made of starch, which is more porous and allows oxygen to seep through its micro-holes. The milk-based packaging, however, has smaller pores and can thus create a tighter network that keeps oxygen out. After a few additional improvements within their research, this casein-based packaging looks similar to store-bought plastic wrap, but it is less stretchy and is better at blocking oxygen.
The material is edible and made almost entirely of proteins. Nutritious additives such as vitamins, probiotics and nutraceuticals could be included in the future. It does not have much taste, the researchers say, but flavorings could be added. In addition to being used as plastic pouches and wraps, this casein coating could be sprayed onto food, such as cereal flakes or bars.
Right now, cereals keep their crunch in milk due to a sugar coating. Instead of all that sugar, manufacturers could spray on casein-protein coatings to prevent soggy cereal. The spray also could line pizza or other food boxes to keep the grease from staining the packaging, or to serve as a lamination step for paper or cardboard food boxes or plastic pouches.
Testing mechanical strength of membranes
Scientists from Mercer University (Macon, GA, USA) have been researching the effect of ablative lasers on in vitro transungal delivery.
They used their TA.XTplus Texture Analyser to measure the mechanical strength of membranes after ablation using a needle penetration technique. The laser was found to disrupt the nail sufficiently to allow for permeation of methotrexate, which is otherwise challenging due to its high molecular weight and low permeability.
Methotrexate is helpful in the treatment of nail psoriasis, so this study is key in showing that transungual methotrexate delivery is enhanced by fractional laser ablation.
Scientists from Queen’s University Belfast have been researching the influence of an alginate backbone on the efficacy of thermo-responsive alginate-g-P(NIPAAm) hydrogel as a vehicle for sustained and controlled gene delivery.
They used their TA.XTplus Texture Analyser to measure the injectability of hydrogel samples. The study developed an injectable and thermo-responsive hydrogel formulation for localised gene delivery.
This helped to find an optimal Alg-g-P(NIPAAm) hydrogel with respect to localised delivery of DNA nanoparticles as a potential medical device for those with castrate resistant prostate cancer.
Lipstick sensory properties
Researchers from Lubrizol Advanced Materials have been investigating the prediction of lipstick sensory properties with lab tests.
Sensory perceptions and performance are important to the success of a lipstick formulation, but in‐vivo evaluation can be expensive and time‐consuming. The goal of this work was to develop and use lab test methods to predict the sensory and performance properties of lipstick.
The researchers used their TA.XTplus Texture Analyser to perform a tack test on the samples. The emollient was found to have a significant effect on the sensory and performance properties of a lipstick, which can be predicted with the developed laboratory tests.
The methods presented may help to speed up the development and optimisation of future lipstick formulations.
Researchers from 3M Corporate Research Materials Laboratory have been investigating the anatomy of the deformation of pressure sensitive adhesives from rigid substrates.
The extent of the deformation of any pressure sensitive adhesive (PSA) during debonding, which is independent if the failure occurs under tensile, shear or peel modes, has been widely recognised as a critical factor determining its capacity to instantly bond, hold a load or resist debonding.
This paper attempts to decouple the three mechanistic steps of the lifetime of a pressure sensitive adhesive, namely bonding, holding, and debonding.
The researchers used their TA.XTplus to obtain debonding profiles in a 90 degree peel testing mode, focussing on the adhesive high strain modulus (as dictated by its crosslinking level), the peel rate and the substrate surface free energy. The experimental results suggest that both substrate surface energetics and bulk properties intrinsic to large deformation of viscoelastic materials must be considered when investigating PSAs debonding phenomena.
Adhesives are used everywhere, but how do we know how good they are or which one to use? Let’s outline some of the methods now used to put tapes through their paces.
The value of the world market for self-adhesive tapes is set to expand at an annual pace of around 6.3% over the next few years, reaching $69 billion by 2022. Opportunities abound across an array of industries, from packaging and non-residential construction to electronics manufacturing.
Proven high performance will allow adhesive tapes to continue to compete against other joining, bonding and sealing technologies. However, as pressure on quality control departments steps up, it is essential to be able to assess accurately adhesive properties and strength to determine the ideal components for a particular tape and so optimise its performance.
3D printing of food
3D printers — machines that can fit on a desktop and create 3D objects from plastics, metals, and other raw materials — can do just about anything.
High-precision jets pump out custom medical implants at the press of a button. Carbon-fibre printers spit out automobile prototypes with jaw-dropping precision. And off-the-shelf modellers generate custom toys, jewellery, home decorations, and clothes with no more than a digital file.
But there’s a new frontier in 3D printing that’s only beginning to come into focus: food. Recent innovations have made possible machines that print, cook, and serve foods on a mass scale. Industry leaders think 3D food printers could improve the nutritional value of meals, produce intricate sculptures out of everyday foodstuff, and solve hunger in regions of the world that lack access to fresh, affordable ingredients. There’s no doubt about it — 3D food printing has come a long way. Here’s the latest in food research that is using 3D printing and the TA.XTplus Texture Analyser to measure the results.
Scientists from The University of Queensland have been researching the optimisation of chocolate 3D printing by correlating thermal and flow properties with 3D structure modelling. They used their TA.XTplus Texture Analyser, along with a custom break probe, to measure the snap force of 3D printed chocolate. The breaking strength of the samples was found to be strongly related to the support structure of the chocolate. This study demonstrated the use of flow enhancer and the inclusion of a support structure in the designed shape were key factors influencing printability capacity of chocolate.
Meanwhile, at the University of Jiangnan, scientists have been investigating the creation of internal structure of mashed potato construct by 3D printing, and its textural properties. Although it is relatively a new area of research, most of the papers about 3D food printing have been focusing on the materials' properties or the printing variables on the 3D printing performance. Previous to this paper, limited information on the modified texture properties of printed samples is available, although the 3D printing technique has the ability to change the internal structure of printed objects by varying infill pattern and infill percentages.
In this study, texture attributes of hardness and gumminess were obtained by texture profile analysis using a TA.XT2 Texture Analyser. The study confirmed that 3D printing has a potential to modify the textural properties of 3D printed samples through varying the infill percentage and the printing paths to fill the object, which possibly provides a novel way of tailoring textural properties of manufactured foods.
Now that 3D-printing technology has become more vital and relevant than ever, Silicon Valley BeeHex has harnessed this technology (funded by a grant from NASA), to 3D print pizza. The purpose of this invention was to create a way for astronauts to select and product delicious food for themselves on missions.
As manned missions to Mars become an ever-increasing possibility, astronauts might be spending much more time in space. To save space-goers from the drudgery of choking down freeze-dried, pre-packaged “space food” day after day, month after month, NASA decided it was time to develop a way to cook in space.
As usual, they will need to make sure that all the key aspects of consumer satisfaction of the resulting printed food are in place and this is where a Texture Analyser comes in!
Researchers from 3M Corporate Research Materials Laboratory have been investigating the anatomy of the deformation of pressure sensitive adhesives from rigid substrates.
The extent of the deformation of any pressure sensitive adhesive (PSA) during debonding, which is independent if the failure occurs under tensile, shear or peel modes, has been widely recognised as a critical factor determining its capacity to instantly bond, hold a load or resist debonding.
This paper attempts to decouple the three mechanistic steps of the lifetime of a pressure sensitive adhesive, namely bonding, holding, and debonding.
The researchers used their TA.XTplus to obtain debonding profiles in a 90 degree peel testing mode, focussing on the adhesive high strain modulus (as dictated by its crosslinking level), the peel rate and the substrate surface free energy. The experimental results suggest that both substrate surface energetics and bulk properties intrinsic to large deformation of viscoelastic materials must be considered when investigating PSAs debonding phenomena.
Adhesives are used everywhere, but how do we know how good they are or which one to use? Let’s outline some of the methods now used to put tapes through their paces.
The value of the world market for self-adhesive tapes is set to expand at an annual pace of around 6.3% over the next few years, reaching $69 billion by 2022. Opportunities abound across an array of industries, from packaging and non-residential construction to electronics manufacturing.
Proven high performance will allow adhesive tapes to continue to compete against other joining, bonding and sealing technologies. However, as pressure on quality control departments steps up, it is essential to be able to assess accurately adhesive properties and strength to determine the ideal components for a particular tape and so optimise its performance.
Research into organically-based films
At The Central University of Venezuela in Caracas, researchers have been researching active and intelligent films made from starchy sources and blackberry pulp.
They used their TA.XT2i Texture Analyser to carry out uniaxial tensile tests on the films. The high toughness of films derived from plantain starch make them extremely useful for packaging, as they could be used to produce films that absorb more energy without this being transmitted to the packaged foods. This could minimise the damage caused by impacts to the food during transport and storage.
Meanwhile, at the Horticultural Crops Technology Research Department, Giza, researchers have been investigating utilisation of orange wastes for production of value added products.
They used their TA.XTplus Texture Analyser to measure the texture of osmotically dehydrated cubes of orange peel. After manufacture, waste from orange juices, concentrates and jam leave 10-15% waste out of the total production.
This waste is a bad source of pollution, insects, and rats especially when left inside factories without removal. This study helped to develop the use of this waste in producing new products.
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Food companies are watching with keen interest as researchers in Japan delve into the nuts and bolts of sensations like "crispness" and "springiness". Their findings are expected to lead to new and more appetising products.
Taste, aroma and appearance are important factors in determining the appeal of foods, but the finer details of the dining experience are still little understood. The researchers are working to uncover the secrets of food texture by gathering data on "mouthfeel" and the microstructures of various ingredients.
Takashi Nakamura, a professor at Meiji University in Tokyo, is conducting studies on the springy textures of various kinds of starch.
Each type has its own characteristics. Tapioca, commonly found in bead-shaped form in Asian milk tea drinks, and "waxy cornstarch," used as a thickener in Japanese sweets, are different forms of starch. Their chewiness is similar, but the "waxy" form is easier to bite through, while tapioca has greater elasticity. The experience of eating them is filtered through the senses, so formulating a numerical index presents a challenge.
Quantifying 'crispy' and 'chewy' points the way to new and better products, according to Rimi Inomata of the Nikkei Asian Review.
Researchers at the Technical University of Denmark have developed a novel, standardised method that can provide a quantitative description of shrimp peelability.
The peeling process was based on the measure of the strength of the shell-muscle attachment of the shrimp using their TA.XTplus Texture Analyser, and calculated into the peeling work. The self-consistent method, insensitive of the shrimp size, was proven valid for assessment of ice maturation of shrimps.
The quantitative peeling efficiency (peeling work) and performance (degree of shell removal) showed that the decrease in peeling work correlated with the amount of satisfactory peeled shrimps, indicating an effective weakening of the shell-muscle attachment.
The developed method provides the industry with a quantitative analysis for measurement of peeling efficiency and peeling performance of shrimps. It may be used for comparing different maturation conditions in relation to optimisation of shrimps peeling.
This is yet another area in which the capabilities of texture analysis help food manufacturers and suppliers understand the detailed properties of their products.
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The boom of 2 billion people over the last century has resulted in an ageing world population.
By 2025, the world will have almost 800 million people over the age of 65. About 556 million of them will be in developing countries, another 254 million in developed ones. In fact, the United Nations estimates that the global population age 60+ will soar from 11% in 2000 to 22% by 2050. While age is just a number, the numbers are certainly on the rise.
Texture is often taken for granted. The acts of chewing (mastication) and swallowing play a huge role not only in nutrient intake, but also in an enjoyable eating experience. This becomes difficult when dental health starts to degrade and salivary flow diminishes. Missing teeth and wearing dentures both impact the act of chewing and decrease biting forces.
Chewing efficiency can also be affected by a decrease in biting and chewing forces attributed to age-related changes in muscle strength. About 40% of elderly people have difficult chewing and swallowing food, and this difficulty has an obvious flow on effect for their health in terms of nutrition, wellbeing, and general quality of life.
Scientists from Ruakura Research Centre have been investigating novel meat-enriched foods for older consumers.
They used their TA.XTplus Texture Analyser to measure bread texture and ice cream meltability. The study helped to develop products that elders could readily consume to meet nutrition requirements and address some of the common ailments associated with aging, such as loss of muscle mass and strength.
Meanwhile, at Université Bourgogne Franche-Comté, scientists have been researching the relationships of oral comfort perception and bolus properties in the elderly for sponge cake and brioche.
They used their TA.XTplus Texture Analyser as a capillary rheometer by equipping it with a cylindrical piston with a capillary die attached to the bottom along with a cylindrical barrel. Boli were loaded into the capillary die immediately after collection from human subjects.
They found that for soft aerated cereal foods, stimulated salivary flow rate is the most important physiological variable that impacts the food bolus properties and the perception of oral comfort in the elderly, even more than the dental status. However, increasing the amount of fat seemed to lower the role of the stimulated flow rate and bolus hydration, likely by increasing lubrication. This highlighted the importance of the hydration and lubrication mechanisms in the oral processing and enjoyment of eating for this type of product in the elderly.
How to make food more palatable while still easy to swallow is an area of ongoing research. By applying rheology, developing new texture models, and looking at the nutrition and swallowing behaviour of foods, a more scientific approach can be brought to the formulation and design of novel texture-modified food.
Looking into edible insect ingredients
At the Institute of Agrochemistry and Food Technology, Valencia, scientists have been investigating insects as ingredients for bakery goods.
Due to a rising demand for proteins, the food industry is considering new alternative protein sources that can be used for human food. The aim of this research was to explore the potential use of insect flour as a protein-rich ingredient for bakery products.
The insects were ground and used to replace 5% of the wheat flour in doughs and breads. This affected rheological properties of the dough during mixing but did not significantly affect specific volume or texture. They used their TA.XTplus Texture Analyser to perform TPA tests on central bread slices.
Meanwhile, scientists from the University of Foggia have been researching the printability, quality and nutritional properties of 3D printed cereal based snacks enriched with edible insects. Mechanical properties of 3D printed snacks were measured using their TA.XTplus Texture Analyser.
Printed snacks reproduced the overall structure of the designed object with sufficient fidelity. However, the addition of different levels of ground larvae of yellow mealworms modified the printability of dough, changing morphological and microstructure properties of raw snacks.
The overall results suggested that together with wheat flour, ground yellow mealworm could be a suitable ingredient to manufacture 3D printed foods with specific designs and improved nutritional quality without adverse impact on technological quality.
Scientists from California State Polytechnic University have also been researching the effects of edible insect ingredients on the physicochemical and sensory properties of extruded rice products. They used their TA.XTplus Texture Analyser to perform hardness and adhesiveness assessments of the samples. Overall, the insect rice was found to have darker colour than the reference brown rice and to be softer and stickier in texture after cooking.
As a staple food providing 20% of the world’s dietary energy and consumed by more than 1 billion people, rice is an ideal vehicle to deliver nutrients carried by edible insects. The incorporation of insect flours in processed foods such as extruded rice products can greatly promote the consumer acceptance by disguising the ‘yuck’ factor associated with intact insects and this study showed that the texture of these products is not adversely affected by incorporating insect ingredients.
Insect innovation: Getting the right flavour and texture for your product is an online article including a report on some Finnish research on the best ways to process mealworms and crickets to get the optimal flavour and texture profile.
Scientists from the Technical University of Munich have been investigating the classification of puffed snacks freshness based on crispiness-related mechanical and acoustical properties.
They used their TA.XTplus Texture Analyser to perform sound-insulated crushing tests on samples equilibrated at different humidity levels. Crispness is a very challenging property to measure using texture analysis alone, and so this study combined 70 different food properties via machine learning algorithms. Sensory panels then ranked crispiness-related freshness and preference based on the recorded sounds.
Selected feature combinations were used to train machine learning models to recognise the freshness levels at different humidity levels. The classification accuracy was improved compared with traditional texture analysis techniques and an accuracy of up to 92% could be achieved.
Scientists from Mustafa Kemal University have been researching the assessment of acoustic-mechanical measurements for the crispness of wafer products. They used their TA.XTplus Texture Analyser along with the Acoustic Envelope Detector to perform mechanical and acoustic fracture measurements on wafer samples – three point bend tests and a craft knife cutting test.
Both tests were found to be able to distinguish acoustic-mechanical properties of wafer products; wafers’ crispness could be differentiated by the parameters of the cutting test and their creaminess was related to mechanical parameters of the three point bend test. Force peaks number and maximum sound pressure showed correlation on both tests.
The study showed that these techniques are capable of differentiating crispy products of different qualities, in different ways.
New advances in transcutaneous delivery
Researchers from Osaka University have been developing novel double-decker microneedle patches for transcutaneous vaccine delivery.
Two types of patch were assessed. Mechanical failure tests were performed with a TA.XTplus Texture Analyser. Each patch was loaded until failure. The required force for mechanical microneedle fracture was measured and the necessary fracture force per needle was calculated by dividing the measured fracture force by the number of fractured needles.
Meanwhile, scientists from Queen’s University Belfast have been investigating novel bilayer dissolving microneedle arrays with concentrated PLGA nanomicroparticles for targeted intradermal delivery. They used their TA.XT2 Texture Analyser to measure the mechanical and insertion properties of nano- and microparticle-loaded microneedle arrays.
These delivery systems continue to receive growing attention due to their ability to bypass the skin's stratum corneum barrier in a minimally-invasive fashion and achieve enhanced transdermal drug delivery and “targeted” intradermal vaccine administration. This study developed a two-stage novel processing strategy to provide a simple and easy method for localising particulate delivery systems into dissolving microneedle arrays.
Researchers from Federal Fluminense University in Brazil have been investigating instrumental texture parameters as freshness indicators in five farmed Brazilian freshwater fish species.
The aim of this study was to assess the chemical quality and instrumental texture parameters of the samples. Texture profile analysis was performed on standardised size fillets using their TA.XTplus Texture Analyser.
They found that with regard to the instrumental texture parameters, firmness, hardness, and chewiness decreased at the beginning of the storage period, whereas an increase was observed in springiness. All instrumental texture parameters demonstrated high correlations with ammonia and TCA-soluble peptides.
The increase in certain biogenic amines (putrescine, cadaverine, and spermine) seems to correlate well with decreases observed in firmness, hardness, and chewiness. In addition, a strong relationship was observed between the initial days of storage and instrumental texture parameters, while a significant correlation between the end of the storage and the chemical quality analyses was verified.
Firmness, hardness, chewiness, and cohesiveness were considered parameters with high potential in the evaluation of fish freshness during the first days of storage, whereas the chemical quality analyses and springiness were considered important for later evaluation of fish quality. Therefore, instrumental texture parameters may be used as quality indicators in the evaluation of freshwater fish freshness.
Texture analysis in determination of 3d printability indicators
The printability of materials used in extrusion based 3D printing is one of the most important properties especially when fabricating objects with architectural complexities.
However, this parameter is influenced by several factors (temperature, components, and additives) which makes thorough evaluation and classification challenging. Researchers at Korea University have been investigating the printability of materials used in extrusion-based 3D printing, which is a very important property, particularly in materials with a complex structure.
Hydrocolloids were used as a reference material to simulate the printability of various types of food applications. After samples were prepared, they were subject to a number of tests including storage and dimensional stability, an assessment of handling properties and a 3D printing test. Additionally, Texture Profile Analysis was carried out using their TA.XTplus Texture Analyser.
The deformation behaviour and handling properties of selected food were classified based on the reference material which enables a printability classification system to be established based on the capability in dimensional stability and degree of handling.
Meanwhile, researchers from Jiangnan University have been investigating lemon juice gel as a food material for 3D printing and optimising printing parameters. Among rheological and NMR tests, texture profile analysis was used, carried out on a TA.XT2 Texture Analyser.
With the increase of starch content, the hardness, springiness, cohesiveness and gumminess of lemon juice gel was increased to different extents, resulting in a stronger ability to resist external damage.
The rheological properties were used as indicators to determine printability and provide basic research on 3D printing for other gel and starch products in this exciting area of new product development.
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